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1.00029

Acetonitrile

≥99.9% (GC), suitable for LC/MS, LiChrosolv®

Acetonitrile

Synonyma:

Methyl cyanide, Anhydrous ACN, Dry MeCN

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1 L
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2 620,00 Kč
2.5 L
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5 490,00 Kč
4 L
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30 L
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185 L
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217 700,00 Kč

O této položce

Lineární vzorec:
CH3CN
Číslo CAS:
Molekulová hmotnost:
41.05
NACRES:
NA.03
EC Index Number:
200-835-2
UNSPSC Code:
12191502
MDL number:
Beilstein/REAXYS Number:
741857
Assay:
≥99.9% (GC)
Technique(s):
HPLC: suitable, LC/MS: suitable
Bp:
81-82 °C (lit.)
Vapor pressure:
72.8 mmHg ( 20 °C), 97 hPa ( 20 °C)

2 620,00 Kč


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Název produktu

Acetonitrile, hypergrade for LC-MS LiChrosolv®

Quality Segment

agency

suitable for ASTM® 7968, suitable for ASTM® 7979, suitable for DIN 38407-42, suitable for EPA 1633, suitable for EPA 8327, suitable for GB 31604.35-2016, suitable for GB 5009.253-2016, suitable for ISO 21675 2019

reg. compliance

suitable for FDA C-010.02

vapor density

1.41 (vs air)

vapor pressure

72.8 mmHg ( 20 °C), 97 hPa ( 20 °C)

product line

LiChrosolv®

assay

≥99.9% (GC)

form

liquid

autoignition temp.

524 °C, 973 °F

expl. lim.

16 %

technique(s)

HPLC: suitable, LC/MS: suitable

impurities

≤0.0001 meq/g Acidity, ≤0.0002 meq/g Alkalinity, ≤0.01% Water, ≤10 ppb Al (Aluminium), ≤10 ppb Ca (Calcium), ≤10 ppb Fe (Iron), ≤10 ppb Mg (Magnesium), ≤5 ppb Any further metal (ICP-MS), ≤5 ppb K (Potassium), ≤50 ppb Na (Sodium)

evapn. residue

≤1.0 mg/L

color

APHA: ≤10

transmittance

191 nm, ≥25%, 195 nm, ≥85%, 200 nm, ≥96%, 215 nm, ≥98%, 230 nm, ≥99%

refractive index

n20/D 1.344 (lit.)

SMILES string

CC#N

bp

81-82 °C (lit.)

mp

−45 °C (lit.)

transition temp

flash point 2 °C

density

0.786 g/mL at 25 °C (lit.)

application(s)

PFAS testing

format

neat

storage temp.

2-30°C

InChI

1S/C2H3N/c1-2-3/h1H3

InChI key

WEVYAHXRMPXWCK-UHFFFAOYSA-N

General description

LiChrosolv hypergrade is accurately tested for LC-MS suitability, and meet all the requirements of modern LC-MS ionization methods (ESI/APCI - positive and negative mode). Thanks to their low level of ionic background and low ion suppression, LiChrosolv hypergrade solvents provide high reproducibility and high ionization efficiency. The packaging material has been improved to meet LC-MS quality requirements perfectly.

Application

Acetonitrile is used as a component:
  • Of the mobile phase in fast LC-MS quantification of illudane glycosides and analogs in bracken ferns.[1]
  • In the elution mixture to extract (fluoro)quinolone antibiotic compounds from the SDB-RPS extraction cartridge.

Preparation Note

Product filtered through a 0.2 μm filter

Other Notes

Explore various lab safety accessories and equipment for safe handling of solvents to increase your safety level from the first usage.

Legal Information

ASTM is a registered trademark of American Society for Testing and Materials
LICHROSOLV is a registered trademark of Merck KGaA, Darmstadt, Germany

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Acetonitrile

Quality Level

100

Quality Level

100

Quality Level

200

Quality Level

200

application(s)

PFAS testing

application(s)

PFAS testing

application(s)

PFAS testing

application(s)

-

assay

≥99.9% (GC)

assay

≥99.8% (GC)

assay

≥99.9% (GC)

assay

≥99.9% (GC)

technique(s)

HPLC: suitable, LC/MS: suitable

technique(s)

HPLC: suitable

technique(s)

-

technique(s)

HPLC: suitable

form

liquid

form

liquid

form

liquid

form

liquid

bp

81-82 °C (lit.)

bp

81-82 °C (lit.)

bp

81-82 °C (lit.)

bp

81-82 °C (lit.)


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pictograms

FlameExclamation mark

signalword

Danger

Hazard Classifications

Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Eye Irrit. 2 - Flam. Liq. 2

Skladovací třída

3 - Flammable liquids

flash_point_f

35.6 °F - closed cup

flash_point_c

2.0 °C - closed cup


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75-05-8

CAS No.


Osvědčení o analýze (COA)

Vyhledejte osvědčení Osvědčení o analýze (COA) zadáním čísla šarže/dávky těchto produktů. Čísla šarže a dávky lze nalézt na štítku produktu za slovy „Lot“ nebo „Batch“.

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Protokoly

Catalyst screening kits, KitAlysis™, and TLC-MS analysis enable high-throughput synthesis and analysis for efficient reactions.

Thin layer chromatography coupled with mass spectrometry does not require substantial sample preparation. Energy drinks can be applied without dilution directly onto the TLC plate.

Qualitative Thin Layer Chromatography Analysis of Flavonoids and Quantification of Terpene Lactones in Ginkgo Biloba Extracts and Tablets

Zobrazit všechny protokoly

Sortimentní položky

Cílem této studie je vyvinout a ověřit metodu LC-ESI-iontové pasti-MS/MS pro identifikaci a kvantifikaci ethylglukuronidu (EtG) a ethylsulfátu (EtS) jako biomarkerů etanolu pro analýzu moči.

Přečtěte si tipy a triky pro výběr a přípravu vhodné pufrové mobilní fáze pro vaše HPLC separace a vývoj metod pro vzorky obsahující ionizovatelné sloučeniny.

Optimize serum samples for LC-MS/MS-based free testosterone determination using Supel™ BioSPME 96-pin device and validated equilibrium dialysis methods.

Zobrazit všechny články

Determination of (fluoro) quinolone antibiotic residues in pig kidney using liquid chromatography-tandem mass spectrometry: I. Laboratory-validated method.
Brigitte T, et al.
Journal of Chromatography A, 1088, 32-39 (2005)
Fast LC-MS quantification of ptesculentoside, caudatoside, ptaquiloside and corresponding pterosins in bracken ferns
Vaidotas K et al.
Journal of Chromatography. B, Analytical Technologies in the Biomedical and Life Sciences, 1138, 121966-121966 (2020)



Globální číslo obchodní položky

Skladová položkaGTIN
100029400004054839365393
100029918504054839495076

Questions

1–2 of 2 Questions  
  1. How can I determine the shelf life / expiration / retest date of this product?

    1 answer
    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/418/501/product-dating-information-06-25-mk.pdf

      Helpful?

  2. How is shipping temperature determined? And how is it related to the product storage temperature?

    1 answer
    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

      Helpful?

Reviews

Active Filters

  1. Gdynia
    • Review 1
    • Votes 7
    5 out of 5 stars.

    Perfect ANC

    At spark-lab we have been using ACN for LC-MS / MS for years. It meets our quality requirements in 100%.

    Helpful?