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Documenti fondamentali

1.03701

Supelco

Hexane

≥99% (GC), suitable for LC/MS, LiChrosolv®

Sinonimo/i:

n-esano

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1 L
133,00 €
2.5 L
257,00 €
4 L
305,00 €

133,00 €


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Cambia visualizzazione
1 L
133,00 €
2.5 L
257,00 €
4 L
305,00 €

About This Item

Formula condensata:
CH3(CH2)4CH3
Numero CAS:
Peso molecolare:
86.18
Beilstein:
1730733
Numero MDL:
Codice UNSPSC:
41116105
Numero indice EU:
203-777-6
NACRES:
NA.03

133,00 €


Per informazioni sulla disponibilità, contatta il Servizio Clienti.

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Nome del prodotto

Esano, hypergrade for LC-MS LiChrosolv®

Densità del vapore

~3 (vs air)

Livello qualitativo

Tensione di vapore

256 mmHg ( 37.7 °C)
5.2 psi ( 37.7 °C)
~132 mmHg ( 20 °C)

Nome Commerciale

LiChrosolv®

Saggio

≥99% (GC)

Stato

liquid

Temp. autoaccensione

453 °F

Limite di esplosione

7.7 %

tecniche

HPLC: suitable
LC/MS: suitable

Impurezze

≤0.0002 meq/g Acidity
≤0.0002 meq/g Alkalinity
≤0.005% Water
≤10 ppb Al (Aluminium)
≤10 ppb Ca (Calcium)
≤10 ppb Fe (Iron)
≤10 ppb Mg (Magnesium)
≤10 ppb Na (Sodium)
≤5 ppb K (Potassium)

Residuo dopo evaporazione

≤2.0 mg/L

Trasmittanza

210 nm, ≥60%
225 nm, ≥90%
245 nm, ≥98%

Indice di rifrazione

n20/D 1.375 (lit.)

Viscosità cinematica

0.50 cSt(20 °C)

P. ebollizione

69 °C (lit.)

Punto di fusione

−95 °C (lit.)

Temp. transizione

flash point -22 °C

Densità

0.659 g/mL at 25 °C (lit.)

Temperatura di conservazione

2-30°C

Stringa SMILE

CCCCCC

InChI

1S/C6H14/c1-3-5-6-4-2/h3-6H2,1-2H3
VLKZOEOYAKHREP-UHFFFAOYSA-N

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Descrizione generale

The product is a high purity solvent that ensures baseline stability, lowest impurity levels and high UV transmittance in LC-MS applications.

Applicazioni

Featured in screening and detection of estrogen-active nonylphenols in water by planar solid-phase extraction followed by high performance thin layer chromatography.
Also used in:
  • analysis of mineral oil saturated hydrocarbons in vegetable oils by LC-GC interface.[1]
  • studies on sugars and organic acids in biological matrices using GC coupled to triple quadruple mass spectrometry (QqQ-MS).[2]

Caratteristiche e vantaggi

  • no ghost peaks
  • full reproducibility
  • extends the lifetime of columns
  • optimized and tested for LC-MS applications
  • minimal background ion suppression
  • reduced risk of contamination
  • less exposure to hazardous chemicals

Nota sulla preparazione

Product filtered through a 0.2 μm filter

Risultati analitici

Purity (GC): ≥ 99.0 %
Identity (IR): conforms
Evaporation residue: ≤ 2.0 mg/l
Water: ≤ 0.005 %
Acidity: ≤ 0.0002 meq/g
Alkalinity: ≤ 0.0002 meq/g
Al (Aluminium): ≤ 10 ppb
Ca (Calcium): ≤ 10 ppb
Fe (Iron): ≤ 10 ppb
K (Potassium): ≤ 5 ppb
Mg (Magnesium): ≤ 10 ppb
Na (Sodium): ≤ 10 ppb
Transmission (at 210 nm): ≥ 60 %
Transmission (at 225 nm): ≥ 90 %
Transmission (from 245 nm): ≥ 98 %
Suitable for LC-MS; Intensity of background mass peak based on reserpine(APCI/ESI positive): ≤ 2 ppb
Suitable for LC-MS; Intensity of background mass peak based on reserpine(APCI/ESI negative): ≤ 20 ppb
Filtered by 0,2 µm filter.

Altre note

Explore various lab safety accessories and equipment for safe handling of solvents to increase your safety level from the first usage.

Note legali

LICHROSOLV is a registered trademark of Merck KGaA, Darmstadt, Germany

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Avvertenze

Danger

Classi di pericolo

Aquatic Chronic 2 - Asp. Tox. 1 - Flam. Liq. 2 - Repr. 2 - Skin Irrit. 2 - STOT RE 2 Inhalation - STOT SE 3

Organi bersaglio

Central nervous system, Nervous system

Codice della classe di stoccaggio

3 - Flammable liquids

Classe di pericolosità dell'acqua (WGK)

WGK 3

Punto d’infiammabilità (°F)

-7.6 °F

Punto d’infiammabilità (°C)

-22 °C


Certificati d'analisi (COA)

Cerca il Certificati d'analisi (COA) digitando il numero di lotto/batch corrispondente. I numeri di lotto o di batch sono stampati sull'etichetta dei prodotti dopo la parola ‘Lotto’ o ‘Batch’.

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Esano HPLC Plus, for HPLC, GC, and residue analysis, ≥95%

Sigma-Aldrich

650552

Esano

Esano for analysis EMPARTA® ACS

Supelco

1.07023

Esano

2-Propanolo hypergrade for LC-MS LiChrosolv®

Supelco

1.02781

2-Propanolo

Esano ReagentPlus®, ≥99%

Sigma-Aldrich

139386

Esano

Quantification of sugars and organic acids in biological matrices using GC-QqQ-MS
Chemosphere, 207-223 (2018)
A lab-developed interface for liquid-gas chromatography coupling based on the use of a modified programmed-temperature-vaporizing injector
Zoccali M, et al.
Journal of Chromatography A, 1622, 461096-461096 (2020)

Articoli

Nonylphenols (NP) are ubiquitous substances that have been detected in highly diverse foodstuff. As breakdown products of nonylphenol ethoxylates, NP could end up in the aquatic environment. This article presents a rapid method for NP detection in surface water by planar solid phase extraction – planar yeast estrogen screen (pSPE-pYES).

Domande

1–2 di 2 domande  
  1. How can I determine the shelf life / expiration / retest date of this product?

    1 risposta
    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/449/386/product-dating-information-mk.pdf

      Utile?

  2. How is shipping temperature determined? And how is it related to the product storage temperature?

    1 risposta
    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

      Utile?

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