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Merck

Development of a rapid and accurate method for the determination of key compounds of pig odor.

Journal of chromatography. A (2004-07-06)
Stephanie Willig, Markus Lacorn, Rolf Claus
RESUMO

Sampling of odor substances in the emissions from swine production facilities is still the limiting step for routine odor quantification. Solid sorption techniques based on cartridges were developed for three categories of substances (indoles, volatile fatty acids and methylthiol) and were standardized to a sampling time of 15 min. These cartridges also trap dust particles which transport odor substances. Quantification was performed by RP-HPLC or GC. Reliability criteria revealed excellent values for sensitivity (lower ppb level) and repeatability (R.S.D. < 10%), thus they are comparable to fiber solid-phase micro extraction sorption techniques. Parallel determinations in feces and air revealed high correlations (r = 0.99, P < 0.01), so that microbial processes during digestion determine odor quality and hence provide a possibility to reduce odor via feeding.

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Conjunto de fibras para SPME de divinilbenzeno-carboxeno-polidimetilsiloxano (DVB/CAR/PDMS), needle size 24 ga, StableFlex
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Conjunto de fibras para SPME de divinilbenzeno-carboxeno-polidimetilsiloxano (DVB/CAR/PDMS), needle size 24 ga, for use with manual holder
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Conjunto de fibras para SPME de divinilbenzeno-carboxeno-polidimetilsiloxano (DVB/CAR/PDMS), needle size 23 ga, StableFlex, for use with autosampler
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Conjunto de fibras para SPME de divinilbenzeno-carboxeno-polidimetilsiloxano (DVB/CAR/PDMS), needle size 23 ga, StableFlex, for use with manual holder or autosampler, fiber L 2 cm
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Conjunto de fibras para SPME de divinilbenzeno-carboxeno-polidimetilsiloxano (DVB/CAR/PDMS), needle size 24 ga, StableFlex, for use with autosampler
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Conjunto de fibras para microextração em fase sólida (SPME) de polidimetilsiloxano (PDMS), df 100 μm(PDMS, needle size 24 ga, for use with manual holder
Supelco
Conjunto de fibras para microextração em fase sólida (SPME) de polidimetilsiloxano (PDMS), df 100 μm(PDMS, for use with autosampler, needle size 23 ga
Supelco
Conjunto de fibras para microextração em fase sólida (SPME) de polidimetilsiloxano (PDMS), df 100 μm(PDMS, for use with autosampler, needle size 24 ga
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Conjunto de fibras de SPME Carboxeno/polidimetilsiloxano (CAR/PDMS), df 75 μm(CAR/PDMS, for use with manual holder, needle size 24 ga
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SPME Fiber Assembly Polydimethylsiloxane/Divinylbenzene (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, StableFlex, for use with autosampler
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Conjunto de fibras de SPME Carboxeno/polidimetilsiloxano (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 23 ga, StableFlex, for use with autosampler
Supelco
SPME Fiber Assembly Polydimethylsiloxane/Divinylbenzene (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, for use with manual holder
Supelco
Conjunto de fibras de SPME Carboxeno/polidimetilsiloxano (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 24 ga, for use with autosampler
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Conjunto de fibras de SPME Carboxeno/polidimetilsiloxano (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 24 ga, StableFlex, for use with autosampler
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Conjunto de fibras para microextração em fase sólida (SPME) de poliacrilato (PA), df 85 μm(PA, for use with autosampler, needle size 23 ga
Supelco
SPME Fiber Assembly Polydimethylsiloxane/Divinylbenzene (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 23 ga, PDMS/DVB StableFlex, for use with autosampler
Supelco
Conjunto de fibras para microextração em fase sólida (SPME) de poliacrilato (PA), df 85 μm(PA, for use with autosampler, needle size 24 ga
Supelco
Conjunto de fibras de SPME Carboxeno/polidimetilsiloxano (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 24 ga, for use with manual holder, StableFlex fiber
Supelco
SPME Fiber Assembly Polydimethylsiloxane/Divinylbenzene (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, StableFlex, for use with manual holder
Supelco
Conjunto de fibras para microextração em fase sólida (SPME) de polidimetilsiloxano (PDMS), df 100 μm(PDMS, for use with manual holder, needle size 23 ga
Supelco
SPME Fiber Assembly Polydimethylsiloxane/Divinylbenzene (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, for use with autosampler
Supelco
Conjunto de fibras de SPME Carboxeno/polidimetilsiloxano (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 23 ga, for use with autosampler
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SPME StableFlex fiber assortment kit, for use with manual holder
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SPME fiber assembly, Carbowax-Polyethylene Glycol (PEG) Coating, needle size 23 ga, df 60 μm(PEG, for use with autosampler
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SPME Fiber Assembly Polydimethylsiloxane/Divinylbenzene (PDMS/DVB), df 65 μm(PDMS/DVB, for use with autosampler, needle size 23 ga
Supelco
Conjunto de fibras de SPME Carboxeno/polidimetilsiloxano (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 23 ga, for use with manual holder
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SPME StableFlex fiber assortment kit, needle size 23 ga, for use with autosampler
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SPME Fiber Assembly Polydimethylsiloxane/Divinylbenzene (PDMS/DVB), fused silica fiber, df 65 μm(PDMS/DVB, for use with manual holder, needle size 23 ga
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SPME fiber assortment kit 4, for use with manual holder, size 24 ga
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Conjunto de fibras para microextração em fase sólida (SPME) de poliacrilato (PA), df 85 μm(PA, for use with manual holder, needle size 24 ga