US EPA Method 8015 (modified): GC Analysis of Gasoline Range Organics (GRO) on SLB®-5ms, Direct Injection
Materiali
Accessorio
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Wheaton wide-mouth bottle
amber soda-lime glass bottle, capacity 1000 mL, white polypropylene cap, (PTFE faced LDPE liner), case of 12 eaBoccole Supeltex M -2B con entrambe le estremità a tronco di cono
I.D. 0.4 mm, 0.10-0.25 mm to like I.D. Column, pkg of 2 eaColonna analitica
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Precolonna
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Standard
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EPA 8270 GC-MS Tuning Solution II
certified reference material, 1000 μg/mL each component in dichloromethaneEPA CLP Semivolatile Calibration Mix
certified reference material, 1000 μg/mL each component in dichloromethane : benzene (3:1)EPA CLP Semivolatiles Surrogate Standards Mix
certified reference material, 4000 μg/mL each component in methylene chlorideEPA 8270 Semivolatile Internal Standard Mix
certified reference material, TraceCERT®, 2000 μg/mL each component in methylene chloride, ampule of 2 × 1 mLEPA 8270 Benzidines Mix
certified reference material, TraceCERT®, 2000 μg/mL each component in methanol, ampule of 1 mLCONDITIONS
column
SLB-5ms, 30 m x 0.25 mm I.D., 1.0 μm (28476-U)
oven
50 °C (3 min), 15 °C/min to 200 °C
inj. temp.
150 °C
detector
FID, 250 °C
carrier gas
helium, 1.3 mL/min., constant
injection
0.5 μL, 50:1 split
liner
2 mm I.D., FocusLiner™ inlet liner
sample
EPA GRO Mix, 9 analytes at various concentrations in methanol (47577-U)
Descrizione
Note legali
FocusLiner is a trademark of SGE Analytical Science Pty Ltd.
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany