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Merck

55227-U

Supelco

Supel QuE QuEChERS tube

Citrate Extraction Tube, pk of 50, suitable for EN 15662

Szinonimák:

QuEChERS

Bejelentkezésa Szervezeti és Szerződéses árazás megtekintéséhez


About This Item

UNSPSC kód:
41115712
NACRES:
NB.21

product name

Supel QuE, Citrate Extraction Tube, pk of 50, suitable for EN 15662

material

polypropylene tube

Minőségi szint

Ügynökség

suitable for EN 15662

termékcsalád

Supel

összetétel

magnesium sulfate, 4 g
sodium chloride, 1 g (Cat. No. S7653)
sodium citrate dibasic sesquihydrate, 0.5 g (Cat. No. 71635)
sodium citrate tribasic dihydrate, 1 g (Cat. No. S4641)

kiszerelés

pk of 50

technika/technikák

QuEChERS: suitable

centrifuga cső térfogata

15 mL

alkalmazás(ok)

food and beverages

elválasztástechnika

ion exchange

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Általános leírás

Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.

Alkalmazás

Supel QuE citrate tube is used for the determination of pesticide residues on vegetables using various analytical techniques.

Alkalmasság

Suitable for extracting ~10 g food/agricultural sample. The citrate is to buffer the extraction to pH 5.0 - 5.5. At this pH, most acid and base labile pesticides are stable.

Jogi információk

Supel is a trademark of Sigma-Aldrich Co. LLC

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Próbálja ki a Termékválasztó eszköz. eszközt

Tárolási osztály kódja

13 - Non Combustible Solids

WGK

WGK 1

Lobbanási pont (F)

Not applicable

Lobbanási pont (C)

Not applicable


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Analitikai tanúsítványok (COA)

Lot/Batch Number

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Dokumentumtár megtekintése

Az ügyfelek ezeket is megtekintették

Monitoring survey of the use patterns and pesticide residues on vegetables in the Niayes zone, Senegal
Diop A, et al.
Chemosphere, 144, 1715-1721 (2016)
Pesticide analysis at ppt concentration levels: coupling nano-liquid chromatography with dielectric barrier discharge ionization-mass spectrometry
Mirabelli.FM, et al.
Analytical and Bioanalytical Chemistry, 408(13), 3425-3434 (2016)
Maria Teresa Salles Trevisan et al.
Journal of chromatography. A, 1512, 98-106 (2017-07-20)
An analytical method using a quick, easy, cheap, effective, rugged and safe (QuEChERS) procedure for multi-residue determination of 52 pesticides in coffee leaf extractshas been developed and validated according to SANTE/11945/2015 guidelines. Different sorbent combinations for dispersive solid phase extraction
Steven J Lehotay et al.
Journal of chromatography. A, 1217(16), 2548-2560 (2010-02-11)
This article describes the comparison of different versions of an easy, rapid and low-cost sample preparation approach for the determination of pesticide residues in fruits and vegetables by concurrent use of gas and liquid chromatography (GC and LC) coupled to
Lijun Han et al.
Analytica chimica acta, 827, 40-46 (2014-05-17)
A new method of sample preparation was developed and is reported for the first time. The approach combines in-vial filtration with dispersive solid-phase extraction (d-SPE) in a fast and convenient cleanup of QuEChERS (quick, easy, cheap, effective, rugged, and safe)

Cikkek

Rapid & accurate analysis of 208 pesticides and their metabolites in a fruit sample using Supel™ QuE QuEChERS mixes for sample preparation and GC-MS/MS.

Pesticide residue analysis of 331 pesticides and 44 metabolites in cabbage samples using Supel™ QuE QuEChERS mixes and Purospher® STAR RP-18e column.

Pistachios 45% fat complicates pesticide analysis. But Z-Sep+ sorbent cleanup after QuEChERS extraction can reduce background for reliable results.

Dual-layer cartridge achieves efficient SPE clean-up for challenging pesticide residue testing in turmeric and spices.

Összes mutatása

Protocols

Normal-phase SPE separates analytes based on polar interaction with sorbents in diverse sample matrices.

Related Content

QuEChERS method simplifies sample cleanup for pesticides analysis in food and agricultural samples.

A szilárd fázisú extrakció megtisztítja a mintákat a kromatográfiás elemzéshez, javítja az adatok minőségét és védi az analitikai oszlopokat.

Solid phase extraction purifies samples for chromatographic analysis, improving data quality and protecting analytical columns.

Chromatograms

application for HPLCapplication for HPLC, application for SPE

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