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Merck

55234-U

Supelco

Supel QuE QuEChERS tube

Acetate Tube, pk of 50, AOAC® 2007.01

Szinonimák:

QuEChERS

Bejelentkezésa Szervezeti és Szerződéses árazás megtekintéséhez


About This Item

UNSPSC kód:
41115712
NACRES:
NB.21

Terméknév

Supel QuE, Acetate Tube, pk of 50, AOAC® 2007.01

material

polypropylene tube

Minőségi szint

Ügynökség

AOAC® 2007.01

termékcsalád

Supel

összetétel

magnesium sulfate, 6 g
sodium acetate, 1.5 g (Cat. No. 58750)

kiszerelés

pk of 50

technika/technikák

QuEChERS: suitable

centrifuga cső térfogata

15 mL

alkalmazás(ok)

food and beverages

elválasztástechnika

ion exchange

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Általános leírás

Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.

Alkalmasság

Suitable for extracting 10-15 g food/agricultural sample. The high level of salts (e.g. magnesium sulfate) is to induce phase separation between the acetonitrile and aqueous sample layer.

Jogi információk

AOAC is a registered trademark of AOAC International
Supel is a trademark of Sigma-Aldrich Co. LLC

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Tárolási osztály kódja

12 - Non Combustible Liquids

WGK

WGK 1

Lobbanási pont (F)

Not applicable

Lobbanási pont (C)

Not applicable


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Analitikai tanúsítványok (COA)

Lot/Batch Number

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Dokumentumtár megtekintése

Az ügyfelek ezeket is megtekintették

Calogero Di Bella et al.
Frontiers in public health, 8, 273-273 (2020-08-01)
Heavy metals and PAHs were measured in animal foodstuffs from Augusta-Melilli-Priolo area in order to evaluate the potential human health risk associated to their consumption. All heavy metals were detected in seafood products while most of them were <LOD in
Steven J Lehotay et al.
Journal of chromatography. A, 1217(16), 2548-2560 (2010-02-11)
This article describes the comparison of different versions of an easy, rapid and low-cost sample preparation approach for the determination of pesticide residues in fruits and vegetables by concurrent use of gas and liquid chromatography (GC and LC) coupled to
Lijun Han et al.
Analytica chimica acta, 827, 40-46 (2014-05-17)
A new method of sample preparation was developed and is reported for the first time. The approach combines in-vial filtration with dispersive solid-phase extraction (d-SPE) in a fast and convenient cleanup of QuEChERS (quick, easy, cheap, effective, rugged, and safe)
Yelena Sapozhnikova et al.
Analytica chimica acta, 758, 80-92 (2012-12-19)
A multi-class, multi-residue method for the analysis of 13 novel flame retardants, 18 representative pesticides, 14 polychlorinated biphenyl (PCB) congeners, 16 polycyclic aromatic hydrocarbons (PAHs), and 7 polybrominated diphenyl ether (PBDE) congeners in catfish muscle was developed and evaluated using
Maria Teresa Salles Trevisan et al.
Journal of chromatography. A, 1512, 98-106 (2017-07-20)
An analytical method using a quick, easy, cheap, effective, rugged and safe (QuEChERS) procedure for multi-residue determination of 52 pesticides in coffee leaf extractshas been developed and validated according to SANTE/11945/2015 guidelines. Different sorbent combinations for dispersive solid phase extraction

Protocols

Analysis of banned neonicotinoid insecticides from dandelion blossoms using QuEChERS and LC-MS.

Normal-phase SPE separates analytes based on polar interaction with sorbents in diverse sample matrices.

Related Content

Gas chromatography separates volatile compounds in the gas phase, applied in various industries for quality control.

QuEChERS method simplifies sample cleanup for pesticides analysis in food and agricultural samples.

Chromatograms

application for SPE, suitable for GCsuitable for GC, application for SPE

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