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Merck

LC/MS/MS of Phospholipids on Ascentis® C18

LC/MS/MS of Phospholipids on Ascentis® C18 application for LC-MS

Materiais

padrão

Nº do produto
Descrição
Preços

1-Palmitoyl-2-oleoyl-sn-glycero-3-phospho-rac-(1-glycerol) ammonium salt

≥99%

L-α-Phosphatidylinositol ammonium salt solution from bovine liver

10 mg/mL in chloroform, ≥98% (TLC)

L-α-Phosphatidylethanolamine, dioleoyl

≥99% (GC), ≥98% (TLC), lyophilized powder

1,2-Dipalmitoyl-rac-glycero-3-phosphocholine

~99%

1,2-Dipalmitoyl-sn-glycero-3-phospho-L-serine sodium salt

≥99% (TLC)

1,2-Dipalmitoyl-sn-glycero-3-phosphate monosodium salt

≥98.0% (TLC)

CONDITIONS

column

Ascentis C18, 15 cm x 2.1 mm I.D., 3 μm particles (581365-U)

mobile phase

10 mM ammonium formate in [A] water; [B] methylene chloride; [C] methanol; (2:3:5, A:B:C)

flow rate

0.2 mL/min

pressure

1270 psi (87 bar)

column temp.

25 °C

detector

MS, ESI(+), MRM as indicated on the figure

injection

2 μL

sample

300 mg/L in mobile phase

Descrição

Nota de análise

An LC/MS/MS is shown here for the separation and detection of phospholipids on an Ascentis C18 reversed-phase column with high separation efficiency and excellent peak shape.

Informações legais

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany