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US EPA Method 8015 (modified): GC Analysis of Gasoline Range Organics (GRO) on SLB®-5ms, Direct Injection

US EPA Method 8015 (modified): GC Analysis of Gasoline Range Organics (GRO) on SLB®-5ms, Direct Injection suitable for GC

Materiais

acessório

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Wheaton wide-mouth bottle

capacity 32 oz (1000 mL), amber, white polypropylene cap, PTFE flat liner

Supeltex M-2B Double-Tapered Ferrule

I.D. 0.4 mm, 0.10-0.25 mm to like I.D. Column, pkg of 2 ea

Capillary Column Butt Connector

body only (ferrules not included)

coluna analítica

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Coluna de GC capilar SLB®-5ms

L × I.D. 30 m × 0.25 mm, df 0.25 μm

Coluna de GC capilar SLB®-5ms

L × I.D. 30 m × 0.25 mm, df 0.50 μm

Coluna de GC capilar SLB®-5ms

L × I.D. 30 m × 0.25 mm, df 1.00 μm

Coluna de GC capilar SLB®-5ms

L × I.D. 20 m × 0.18 mm, df 0.18 μm

padrão

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N-Nitrosodiphenylamine solution

certified reference material, 5000 μg/mL in methanol

Perfluorotributylamine (PFTBA)

analytical standard

EPA 8270 GC-MS Tuning Solution II

certified reference material, 1000 μg/mL each component in dichloromethane

EPA GRO Mix

certified reference material, in methanol (varied)

EPA CLP Semivolatile Calibration Mix

certified reference material, 1000 μg/mL each component in dichloromethane : benzene (3:1)

EPA CLP Semivolatiles Surrogate Standards Mix

certified reference material, 4000 μg/mL each component in methylene chloride

EPA 8270 Semivolatile Internal Standard Mix

certified reference material, TraceCERT®, 2000 μg/mL each component in methylene chloride, ampule of 2 × 1 mL

EPA 8270 Benzidines Mix

certified reference material, TraceCERT®, 2000 μg/mL each component in methanol, ampule of 1 mL

pré-coluna

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Intermediate Polar Fused Silica Tubing

L × I.D. 5.0 m × 0.25 mm

CONDITIONS

column

SLB-5ms, 30 m x 0.25 mm I.D., 1.0 μm (28476-U)

oven

50 °C (3 min), 15 °C/min to 200 °C

inj. temp.

150 °C

detector

FID, 250 °C

carrier gas

helium, 1.3 mL/min., constant

injection

0.5 μL, 50:1 split

liner

2 mm I.D., FocusLiner inlet liner

sample

EPA GRO Mix, 9 analytes at various concentrations in methanol (47577-U)

Descrição

Informações legais

FocusLiner is a trademark of SGE Analytical Science Pty Ltd.
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany