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GC Analysis of Trichloroanisole (TCA) in Wine on SLB®-5ms after SPME using 100 μm PDMS Fiber

GC Analysis of Trichloroanisole (TCA) in Wine on SLB®-5ms after SPME using 100 μm PDMS Fiber suitable for GC, application for SPME

Materiais

Fibra para SPME

Nº do produto
Descrição
Preços

57928-U

Conjunto de fibras para microextração em fase sólida (SPME) de polidimetilsiloxano (PDMS)

metal alloy fiber, df 100 μm(PDMS, needle size 23 ga, for use with autosampler

coluna analítica

Nº do produto
Descrição
Preços

28471-U

Coluna de GC capilar SLB®-5ms

L × I.D. 30 m × 0.25 mm, df 0.25 μm

padrão

Nº do produto
Descrição
Preços

47526-U

2,4,6-Trichloroanisole solution

certified reference material, 100 μg/mL in methanol

CONDITIONS

sample/matrix

red wine spiked with 5 ppt TCA

SPME fiber

100 μm PDMS metal fiber (57928-U)

extraction

headspace, room temp (30 min)

condition

3 min. at 250 °C

desorption process

250 °C for 3 min

column

SLB®-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)

oven

60 °C (2 min), 8 °C/min to 200 °C (10 min)

MSD interface

300 °C

scan range

SIM, m/z = 195, 197, 210, 212

carrier gas

helium, 1 mL/min. constant

liner

0.75 mm I.D. SPME

Descrição

Informações legais

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Related Product Categories

HPLC ColumnsGC Columns & AccessoriesTLC Plates & AdsorbentsSolid Phase Microextraction (SPME)Solid Phase Extraction & QuEChERS

Related Applications

Small Molecule HPLCLarge Molecule HPLCGas Chromatography (GC)TLCSolid Phase Microextraction (SPME)Solid Phase Extraction (SPE)QuEChERS