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Amberlite XAD®-2

pkg of 500 g

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About This Item

Número CAS:
Número MDL:
Código UNSPSC:
23151817
Preço e disponibilidade não estão disponíveis no momento.

Agency

suitable for ASTM® D4861
suitable for EPA Method 10A, Method 23 and OTM-45

Formulário

beads (small)

embalagem

pkg of 500 g

técnica(s)

HPLC: suitable
LPLC: suitable

área da superfície

~300 m2/g

Matriz

styrene-divinylbenzene (macroreticular)

Grupo ativo da matriz

polymer

tamanho de partícula

20-60 mesh

tamanho de poro

~0.65 mL/g pore volume
90 Å mean pore size

densidade

1.02 g/mL at 25 °C (true wet)(lit.)
1.08 g/mL at 25 °C (skeletal)(lit.)

técnica de separação

reversed phase

temperatura de armazenamento

2-8°C

cadeia de caracteres SMILES

N([C@@H](CCC(=O)OC(C)(C)C)C=O)C(=O)OCC1c2c(cccc2)c3c1cccc3

InChI

1S/C24H27NO5/c1-24(2,3)30-22(27)13-12-16(14-26)25-23(28)29-15-21-19-10-6-4-8-17(19)18-9-5-7-11-20(18)21/h4-11,14,16,21H,12-13,15H2,1-3H3,(H,25,28)/t16-/m0/s1

chave InChI

BCIPGSZQUDLGSY-INIZCTEOSA-N

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Descrição geral

Amberlite XAD-2, um copolímero hidrofóbico da resina estireno-divinilbenzeno, requer um processo de purificação mais longo e é usado como sorvente. A resina Amberlite XAD-2, dependendo da aromaticidade e do tamanho dos grupos hidrofóbicos, absorve compostos orgânicos por meio de interações físicas de baixa energia.[1]
Resina macrorreticular não iônica que adsorve e libera espécies iônicas por meio de interações hidrofóbicas e polares; geralmente usada em condições isocráticas.
Especificações:

Aplicação

Foi usada a Amberlite XAD®-2:
  • como adsorvente na extração de compostos organoclorados usando a técnica de extração Soxhlat[1]
  • como adsorvente na extração de amostras de mel usando a cromatografia em coluna para análise por HPLC[2]
  • na cromatografia de adsorção[3]
Resina adsorvente poliaromática para compostos hidrofóbicos de PM de até 20.000: fenóis, remoção orgânica, tensoativos, compostos aromáticos, recuperação de antibióticos. Pode ser usado como suporte para catalisadores ou remoção de metais. Para versões limpas de acordo com a Agência de proteção ambiental (EPA) dos EUA, vide Supelpak-2 e Supelpak-2B.
     

Informações legais

ASTM is a registered trademark of American Society for Testing and Materials
Amberlite is a trademark of DuPont de Nemours, Inc.
XAD is a registered trademark of The Dow Chemical Company or an affiliated company of Dow

produto relacionado

Nº do produto
Descrição
Preços

Código de classe de armazenamento

11 - Combustible Solids

Classe de risco de água (WGK)

WGK 3

Ponto de fulgor (°F)

Not applicable

Ponto de fulgor (°C)

Not applicable

Equipamento de proteção individual

Eyeshields, Gloves, type N95 (US)


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Certificados de análise (COA)

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Xinghui Xia et al.
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The Journal of toxicological sciences, 35(6), 817-826 (2010-12-09)
Amberlite XAD-2 resin extracts of river and drinking water sampled from the Northwest district of Chiba Prefecture in each month during the period from January to December 2008 were investigated to characterize and determine their mutagenic potentials and polycyclic aromatic
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The adsorption of SPADNS (trisodium salt of 2-(p-sulfophenylazo)-1,8-dihydroxynaphthalene-3,6-disulfonic acid) onto resins XAD 2, XAD 7 and silica gel was studied in the presence and in the absence of the cationic surfactant CTAB (cetyl trimethylammonium bromide). At a ratio of 2.5
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Two novel azocalix[4]pyrrole Amberlite XAD-2 polymeric chelating resins were synthesized by covalently linking diazotized Amberlite XAD-2 with calix[4]pyrrole macrocycles. The chelating resins were used for extraction, preconcentration and sequential separation of metal ions such as Cu(II), Zn(II) and Cd(II) by

Conteúdo relacionado

A cromatografia líquida de baixa pressão (LPLC) é uma técnica cromatográfica que opera com baixas pressões para impulsionar a fase móvel para a coluna que contém uma fase estacionária por meio da ação de uma bomba.

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Questions

1–7 of 7 Questions  
  1. How can I determine the shelf life / expiration / retest date of this product?

    1 answer
    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/449/386/product-dating-information-mk.pdf

      Helpful?

  2. How is shipping temperature determined? And how is it related to the product storage temperature?

    1 answer
    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

      Helpful?

  3. What is the most approriate protocol to wash Amberlite before use? Thanks in advance!

    1 answer
    1. Amberlite XAD-2 is a crude preparation and must be thoroughly cleaned prior to use.

      1. Rinse with hot deionized water (may hold in nylon filter cloth to retain particles) - use at least 3 bed volumes per hour at 110 deg C
      2. Soak overnight in 2 bed volumes (BV) of ethanol.
      3. Load resin into a glass column and rinsed with a further 2 BV of ethanol.
      4. Rinse with 2 BV of deionized water to remove the ethanol, 1 BV of 4% (w/v) sodium hydroxide, 2 BV of deionized water, 1 BV 4% (v/v) hydrochloric acid, and finally rinse with deionized water until the pH of the eluent is neutral.

      For further use it is advantageous to do a wash in the same solvent use in the application.
      Store in sealed container; may be refrigerated but NOT frozen. As a bacteriostat, one may rinse with 20% ethanol (deionized water) prior to storage.

      Helpful?

  4. What is the Department of Transportation shipping information for this product?

    1 answer
    1. Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product.

      Helpful?

  5. Do you offer a precleaned Amberlite XAD-2?

    1 answer
    1. Yes.  Supelco cleans Amberlite XAD2 for a variety of environmental applications.

      Helpful?

  6. May I purchase Amberlite XAD-2 in large quantities?

    1 answer
    1. The largest package size of Amberlite XAD2 is 25 kg (Product No. 3025-U).

      Helpful?

  7. Is Amberlite XAD-2 ready-to-use?

    1 answer
    1. No.  Amberlite XAD2 is shipped imbibed with 5% NaCl & 1% NaCO3; it has not been specially processed nor cleaned. We suggest that it be extensively treated to a suitable preliminary elution and wash.

      Helpful?

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