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55234-U

Supelco

Supel™ QuE QuEChERS tube

Acetate Tube, pk of 50, AOAC® 2007.01

Synonim(y):

QuEChERS

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About This Item

Kod UNSPSC:
41115712
NACRES:
NB.21

product name

Supel™ QuE, Acetate Tube, pk of 50, AOAC® 2007.01

Materiały

polypropylene tube

agency

AOAC® 2007.01

linia produktu

Supel™

skład

magnesium sulfate, 6 g
sodium acetate, 1.5 g (Cat. No. 58750)

opakowanie

pk of 50

metody

QuEChERS: suitable

pojemność probówki reakcyjnej (do wirowania)

15 mL

Zastosowanie

food and beverages

metoda separacji

ion exchange

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Opis ogólny

Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.

Przydatność

Suitable for extracting 10-15 g food/agricultural sample. The high level of salts (e.g. magnesium sulfate) is to induce phase separation between the acetonitrile and aqueous sample layer.

Informacje prawne

AOAC is a registered trademark of AOAC International
Supel is a trademark of Sigma-Aldrich Co. LLC

Kod klasy składowania

12 - Non Combustible Liquids

Klasa zagrożenia wodnego (WGK)

WGK 1

Temperatura zapłonu (°F)

Not applicable

Temperatura zapłonu (°C)

Not applicable

Choose from one of the most recent versions:

Certyfikaty analizy (CoA)

Lot/Batch Number
18849202
18849201
18707101
18566801
18321101

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Calogero Di Bella et al.
Frontiers in public health, 8, 273-273 (2020-08-01)
Heavy metals and PAHs were measured in animal foodstuffs from Augusta-Melilli-Priolo area in order to evaluate the potential human health risk associated to their consumption. All heavy metals were detected in seafood products while most of them were <LOD in
Lijun Han et al.
Analytica chimica acta, 827, 40-46 (2014-05-17)
A new method of sample preparation was developed and is reported for the first time. The approach combines in-vial filtration with dispersive solid-phase extraction (d-SPE) in a fast and convenient cleanup of QuEChERS (quick, easy, cheap, effective, rugged, and safe)
Steven J Lehotay et al.
Journal of chromatography. A, 1217(16), 2548-2560 (2010-02-11)
This article describes the comparison of different versions of an easy, rapid and low-cost sample preparation approach for the determination of pesticide residues in fruits and vegetables by concurrent use of gas and liquid chromatography (GC and LC) coupled to
M Picot Groz et al.
The Science of the total environment, 493, 162-169 (2014-06-20)
The UV filters and musk fragrances have come into focus because these compounds are contained and increasingly used not only in sunscreen products but also in many products of daily use, such as cosmetics, skin creams, plastics or varnish. In
Yelena Sapozhnikova et al.
Analytica chimica acta, 758, 80-92 (2012-12-19)
A multi-class, multi-residue method for the analysis of 13 novel flame retardants, 18 representative pesticides, 14 polychlorinated biphenyl (PCB) congeners, 16 polycyclic aromatic hydrocarbons (PAHs), and 7 polybrominated diphenyl ether (PBDE) congeners in catfish muscle was developed and evaluated using
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Protokoły

Neonicotinoids Ban: Impact on Plant Material

Analysis of banned neonicotinoid insecticides from dandelion blossoms using QuEChERS and LC-MS.

Solid Phase Extraction: Normal Phase Methodology

Normal-phase SPE separates analytes based on polar interaction with sorbents in diverse sample matrices.

Powiązane treści

Gas Chromatography (GC)

Gas chromatography separates volatile compounds in the gas phase, applied in various industries for quality control.

Chromatografia gazowa (GC)

Chromatografia gazowa oddziela lotne związki w fazie gazowej, stosowane w różnych gałęziach przemysłu do kontroli jakości.

QuEChERS Sample Prep Method

QuEChERS method simplifies sample cleanup for pesticides analysis in food and agricultural samples.

Metoda przygotowania próbki QuEChERS

Metoda QuEChERS upraszcza oczyszczanie próbek do analizy pestycydów w próbkach żywności i rolniczych.

Chromatograms

application for SPE, suitable for GCsuitable for GC, application for SPE

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