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55288-U

Supelco

Supel™ QuE QuEChERS tube

PSA/C18 Tube, pack of 100, AOAC® 2007.01

Synonim(y):

QuEChERS

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About This Item

Kod UNSPSC:
41115712
NACRES:
NB.21

product name

Supel™ QuE, PSA/C18 Tube, pack of 100, AOAC® 2007.01

Materiały

polypropylene tube

agency

AOAC® 2007.01

linia produktu

Supel™

skład

Discovery® DSC-18, 50 mg
magnesium sulfate, 150 mg
Supelclean PSA, 50 mg

opakowanie

pack of 100

metody

QuEChERS: suitable

pojemność probówki reakcyjnej (do wirowania)

2 mL

grupa aktywna macierzy

C18 phase
PSA phase

Zastosowanie

food and beverages

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Opis ogólny

Dispersive SPE (dSPE), often referred to as the "QuEChERS" method (Quick, Easy, Cheap, Effective, Rugged, and Safe), is modern sample prep technique that is becoming increasingly popular in the area of multi-residue pesticide analysis in food and agricultural products.

Using the QuEChERS method, food/agricultural samples are first extracted with an aqueous miscible solvent (e.g., acetonitrile) in the presence of high amounts of salts (e.g., sodium chloride and magnesium sulfate) and/or buffering agents (e.g. citrate) to induce liquid phase separation and stabilize acid and base labile pesticides, respectively. Upon shaking and centrifugation, an aliquot of the organic phase is subjected to further cleanup using SPE. Unlike traditional methods using SPE tubes, in dispersive SPE, cleanup is facilitated by mixing bulk amounts of SPE (e.g., Supelclean PSA, ENVI-Carb, and/or Discovery DSC-18) with the extract. After sample cleanup, the mixture is centrifuged and the resulting supernatant can either be analyzed directly or can be subjected to minor further treatment before analysis.

Supelco carries a line of vials and centrifuge tubes containing pre-determined amounts of salts and SPE sorbents to support the most common method configurations used today.

Informacje prawne

AOAC is a registered trademark of AOAC International
Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany
Supel is a trademark of Sigma-Aldrich Co. LLC

Kod klasy składowania

13 - Non Combustible Solids

Klasa zagrożenia wodnego (WGK)

WGK 3

Temperatura zapłonu (°F)

Not applicable

Temperatura zapłonu (°C)

Not applicable

Choose from one of the most recent versions:

Certyfikaty analizy (CoA)

Lot/Batch Number
17237501
15918001
12586901
11881801
10248801

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Steven J Lehotay et al.
Journal of chromatography. A, 1217(16), 2548-2560 (2010-02-11)
This article describes the comparison of different versions of an easy, rapid and low-cost sample preparation approach for the determination of pesticide residues in fruits and vegetables by concurrent use of gas and liquid chromatography (GC and LC) coupled to
Lijun Han et al.
Analytica chimica acta, 827, 40-46 (2014-05-17)
A new method of sample preparation was developed and is reported for the first time. The approach combines in-vial filtration with dispersive solid-phase extraction (d-SPE) in a fast and convenient cleanup of QuEChERS (quick, easy, cheap, effective, rugged, and safe)
Yelena Sapozhnikova et al.
Analytica chimica acta, 758, 80-92 (2012-12-19)
A multi-class, multi-residue method for the analysis of 13 novel flame retardants, 18 representative pesticides, 14 polychlorinated biphenyl (PCB) congeners, 16 polycyclic aromatic hydrocarbons (PAHs), and 7 polybrominated diphenyl ether (PBDE) congeners in catfish muscle was developed and evaluated using
David Moreno-González et al.
Talanta, 128, 299-304 (2014-07-26)
In this study a fast, selective and sensitive multiresidue method based on QuEChERS methodology has been evaluated and validated for the determination of carbamate pesticides, in edible vegetable oils by UHPLC-MS/MS. A new clean-up sorbent, Supel(TM) QuE Z-Sep(+), has been
Lijun Han et al.
Journal of separation science, 39(23), 4592-4602 (2016-11-03)
A novel carbon/zirconia-based material, Supel
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Protokoły

Neonicotinoids Ban: Impact on Plant Material

Analysis of banned neonicotinoid insecticides from dandelion blossoms using QuEChERS and LC-MS.

Powiązane treści

Supel™ QuE Z-Sep Sorbents for QuEChERS

Z-Sep sorbents improve fat and pigment extraction in QuEChERs solid phase extraction for sample preparation.

Chromatograms

application for HPLCapplication for HPLC, application for SPE

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