US EPA Method 0030: GC Analysis of Volatiles on SPB®-624 after Collection/Desorption using VOST 100 Tube
CONDITIONS
sample
calibration standard: volatiles in methanol; blank: Tenax TA tube with surrogate thermally desorbed into purge & trap system
adsorbent tube
VOST 100 (20074-U)
purge trap
VOCARB 4000 (20308)
column
SPB-624, 75 m × 0.53 mm I.D., 3.0 μm film (25432)
oven
35 °C (5 min) to 200 °C at 10 °C/min, hold 2 min
detector
FID, 300 °C
carrier gas
helium, 8 mL/min
Descrição
Informações legais
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany