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GC Analysis of Volatiles in Water on SPB®-1 after SPME using 100 μm PDMS Fiber

GC Analysis of Volatiles in Water on SPB®-1 after SPME using 100 μm PDMS Fiber suitable for GC, application for SPME

Materiais

Fibra para SPME

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Preços

Conjunto de fibras para microextração em fase sólida (SPME) de polidimetilsiloxano (PDMS)

df 100 μm(PDMS, needle size 24 ga, for use with manual holder

coluna analítica

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SPB®-1 Capillary GC Column

L × I.D. 10 m × 0.20 mm, df 1.20 μm

CONDITIONS

SPME fiber

polydimethylsiloxane, 100 μm (57300-U)

extraction

5 min immersed in water with rapid stirring

column

SPB-1, 10 m × 0.20 mm I.D., 1.2 μm (24134-U)

oven

40 °C ( 0.75 min) to 160 °C at 20 °C/min

inj. temp.

230 °C, splitless (closed 3 min)

detector

FID, 260 °C

carrier gas

helium, 40 cm/sec

sample

50ppb each analyte in 1.8 mL saturated salt water

Descrição

Informações legais

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany