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Documentos

23184

Sigma-Aldrich

Cloreto de Fmoc

BioReagent, ≥99.0% (HPLC)

Sinônimo(s):

Cloreto de 9-fluorenilmetoxicarbonila, Cloroformato de 9-fluorenilmetila, Fmoc-Cl

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About This Item

Fórmula empírica (Notação de Hill):
C15H11ClO2
Número CAS:
28920-43-6
Peso molecular:
258.70
Beilstein:
2279177
Número CE:
249-313-6
Número MDL:
MFCD00001138
Código UNSPSC:
12352108
ID de substância PubChem:
329752391
NACRES:
NA.22

linha de produto

BioReagent

Ensaio

≥99.0% (HPLC)

forma

solid

pf

61-64 °C
62-64 °C (lit.)

grupo funcional

Fmoc

temperatura de armazenamento

2-8°C

cadeia de caracteres SMILES

ClC(=O)OCC1c2ccccc2-c3ccccc13

InChI

1S/C15H11ClO2/c16-15(17)18-9-14-12-7-3-1-5-10(12)11-6-2-4-8-13(11)14/h1-8,14H,9H2

chave InChI

IRXSLJNXXZKURP-UHFFFAOYSA-N

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Aplicação

9-Fluorenylmethoxycarbonyl chloride (Fmoc-Cl) is a reagent for pre-column derivatization of amino acids and biogenic amines for HPLC amino acid analysis and for preparing N-Fmoc amino acids for solid-phase peptide synthesis.
Reagente para derivatização de aminoácidos para análise de aminoácidos por HPLC e para preparo de aminoácidos N-Fmoc para síntese de peptídeos em fase sólida.

Outras notas

Reagent for the pre-column fluorescent derivatization of amino acids

Pictogramas

Corrosion
GHS05

Palavra indicadora

Danger

Frases de perigo

H314

Classificações de perigo

Eye Dam. 1 - Skin Corr. 1B

Perigos de suplementos

EUH029

Código de classe de armazenamento

8A - Combustible corrosive hazardous materials

Classe de risco de água (WGK)

WGK 3

Ponto de fulgor (°F)

Not applicable

Ponto de fulgor (°C)

Not applicable

Equipamento de proteção individual

Eyeshields, Faceshields, Gloves, type P3 (EN 143) respirator cartridges

Certificados de análise (COA)

Busque Certificados de análise (COA) digitando o Número do Lote do produto. Os números de lote e remessa podem ser encontrados no rótulo de um produto após a palavra “Lot” ou “Batch”.

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Supelco

76737

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1,8-Diazafluoren-9-one

Sigma-Aldrich

33484

1,8-Diazafluoren-9-one

Ftaldialdeído suitable for HPLC fluorimetric detection of amino acids, ≥99% (HPLC), powder or crystals

Sigma-Aldrich

P0657

Ftaldialdeído

E J Miller et al.
Analytical biochemistry, 190(1), 92-97 (1990-10-01)
A recently described procedure for amino acid analyses has been modified and adapted for use in quantitating the unique mixture of products commonly found in hydrolysates of the collagens. The method involves precolumn derivatization of hydrolysates with 9-fluorenylmethyl chloroformate (FMOC-CL)
Ibolya Molnár-Perl
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 879(17-18), 1241-1269 (2011-03-05)
An overview is presented on the advancement of the two most frequently used derivatization protocols applying the o-phthalaldehyde (OPA)-thiol and the fluorenylmethyloxycarbonyl (FMOC) chloride reagents, prior to the high performance liquid chromatographic analysis of amino acids. This review pays special
Valentin Lozanov et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 860(1), 92-97 (2007-11-07)
A liquid chromatography method for simultaneous analysis of amino acids, polyamines, catecholeamines and metanephrines in human body fluids after derivatization with 9-fluorenylmethyloxycarbonyl chloride was developed. The chromatographic behavior of analytes at different pH of mobile phase was studied. Successful baseline
P Fürst et al.
Journal of chromatography, 499, 557-569 (1990-01-19)
Reversed-phase high-performance liquid chromatography (RP-HPLC) is a powerful method for assaying physiological amino acid concentrations in biological fluids. Four pre-column derivatization methods, with o-phthaldialdehyde (OPA), 9-fluorenylmethyl chloroformate (FMOC-Cl), phenyl isothiocyanate (PITC) and 1-dimethylaminonaphthalene-5-sulphonyl chloride (dansyl-Cl), were assessed with respect to
A Jámbor et al.
Journal of chromatography. A, 1216(34), 6218-6223 (2009-07-28)
This paper, as a novelty to this field, presents the deproteinization and derivatization of plasma's free amino acids (PFAAs), simultaneously, in a single step, with the acetonitrile (ACN) containing 9-fluorenylmethyloxycarbonyl chloride (FMOC) reagent. Deproteinization and derivatization, were studied with 22
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