1.15037

HPTLC plates, Silica gel 60 RP-18 with concentrating zone 20 x 2.5 cm

pkg of 25 plates, plate L × W 20 mm × 10 cm, according to DIN 38409-H13, glass support

• Sinônimo(s): High Performance TLC Plates
• Código UNSPSC: 41115711

Propriedades

• Materiais: glass support; silica gel 60 matrix
• Nível de qualidade: 100
• Agency: according to DIN 38409-H13
• Características: binder Organic Polymer; fluorescent indicator: no
• classe(s) química(is) do analito: PAHs
• embalagem: pkg of 25 plates
• técnica(s): HPTLC: suitable
• espessura da camada: 150-200 μm
• placa C × L: 20 mm × 10 cm
• tamanho de partícula: 5-6 μm
• tamanho de poro: 60 Å medium pore diameter
• temperatura de armazenamento: 2-30°C

Descrição

Descrição geral

25 Glass plates 20 x 10 cm for PAH determination acc. to DIN 38409-H13

These plates allow users to quickly and easily apply any kind of sample, even large volumes of diluted samples. Our concentrating zone plates are based on different adsorption properties of two adsorbents. The first is a large pore concentrating adsorbent where the samples are applied; the second is a selective layer for separation. Regardless of the spots’ shape, size, or position, the sample always concentrates as a narrow band where the two adsorbents overlap and where the separation starts. These plates allow users to quickly and easily apply any kind of sample, even large volumes of diluted samples.

Ligação

Replaces: 15037-6; 15037

Nota de análise

Specific surface area (according to BET; 5-Pt. measurement): 480 - 540 m²/g
Pore volume (N₂-isotherm): 0.74 - 0.84 ml/g
d 50 (laser diffraction, size distribution): 5 - 7 µm
Layer thickness: 150 - 200 µm
Deviation of layer thickness per plate: ≤ 35 µm
layer thickness concentrating zone: 70 - 110 µm
Fluctuation in the thickness of the concentration zone: ≤ 35 µm
Chromatographic testings:
A) cholesterin test
hRf-values
- cholesterin, cholesterin test:
11 - 23
B) Steroide test
- methyltestosterone, steroid test: 20 - 40
- Reichstein S, steroid test: 50 - 70
- hydrocortisone, steroid test: 65 - 85
Typical value determined on a activated plate (120°C, 15 min)
Eluent a) acetone/ water (95/5 v/v)
Eluent b) acetonitrile/ water (70/30 v/v)