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TLC Analysys of Antioxidative Flavonoids in Plant Extracts on Silica Gel 60 F254s

TLC Analysys of Antioxidative Flavonoids in Plant Extracts on Silica Gel 60 F254s application for TLC

Materiali

Accessorio

N° Catalogo
Descrizione
Determinazione del prezzo

Bottle-type sprayer

capacity 240 mL

Rectangular TLC developing tanks, complete

L × H × W 27.0 cm × 26.5 cm × 7.0 cm

Sigma TLC spray box

Spectroline® E-Series UV lamp

output8 W, AC/DC input 115 V AC

Rectangular TLC developing tanks, complete

L × H × W 7.5 cm × 15.5 cm × 8.0 cm

Hamilton® TLC syringes

1702, volume 25 μL, needle size 22s ga, needle L 51 mm (2 in.),

coated tip

Spectroline® E-Series UV lamp

output6 W, AC/DC input 120 V AC

Hamilton® TLC syringes

1705, volume 50 μL, needle size 22 ga, needle L 51 mm (2 in.),

coated tip

Hamilton® TLC syringes

1701, volume 10 μL, needle size 26s ga, needle type, fixed, needle L 51 mm (2 in.),

coated tip

Rectangular TLC developing tanks, complete

L × H × W 17.5 cm × 16.0 cm × 8.2 cm

Spectroline® E-Series UV lamp

output6 W, AC/DC input 230 V AC

Spectroline® E-Series UV lamp

output4 W, AC/DC input 230 V AC

Spectroline® E-Series UV lamp

output8 W, AC/DC input 230 V AC

Latch-lid TLC developing chambers

For use with 10 cm × 10 cm plates

Hamilton® TLC syringes

1710, volume 100 μL, needle size 22 ga, needle L 51 mm (2 in.),

coated tip

Latch-lid TLC developing chambers

For use with 20 cm × 20 cm plates

Spectroline® E-Series UV lamp

output4 W, AC/DC input 115 V AC

Kimble® microcapillary pipettes

Kimble® microcapillary pipettes

Kimble® microcapillary pipettes

capacity 20 μL, accuracy: ±0.5%

Reagent sprayer for TLC plates

volume 250 mL, Bottle-Type

CONDITIONS

sample preparation

Extract samples were filtered with a 0.45 μm syringe filter. Application by CAMAG ATS4 6mm bandwise.

plate

1.15445 HPTLC LiChrospher Silica gel 60 F254s 20 cm x 10 cm (1.15445.0001)

eluent

[A] ethylacetate; [B] formic acid; [C] glacial acid; [D] water; (100:11:11:27, A:B:C:D) containing 0.1% n-Heptane

migration distance

5 cm

chamber

normal chamber without chamber saturation

detector

366 nm Diphenylboric acid-2-aminoethylester-reagent for Flavonoids, Vanillin-sulfuric acidreagent e.g. for Phenols, Steroids, Glycoside; DPPH reagent for antioxidants (visible light)