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Merck

Development of a rapid and accurate method for the determination of key compounds of pig odor.

Journal of chromatography. A (2004-07-06)
Stephanie Willig, Markus Lacorn, Rolf Claus
ABSTRACT

Sampling of odor substances in the emissions from swine production facilities is still the limiting step for routine odor quantification. Solid sorption techniques based on cartridges were developed for three categories of substances (indoles, volatile fatty acids and methylthiol) and were standardized to a sampling time of 15 min. These cartridges also trap dust particles which transport odor substances. Quantification was performed by RP-HPLC or GC. Reliability criteria revealed excellent values for sensitivity (lower ppb level) and repeatability (R.S.D. < 10%), thus they are comparable to fiber solid-phase micro extraction sorption techniques. Parallel determinations in feces and air revealed high correlations (r = 0.99, P < 0.01), so that microbial processes during digestion determine odor quality and hence provide a possibility to reduce odor via feeding.

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Gruppo in fibra SPME divinilbenzene/carbossene/polidimetilsilossano (DVB/CAR/PDMS), needle size 24 ga, StableFlex
Supelco
Gruppo in fibra SPME divinilbenzene/carbossene/polidimetilsilossano (DVB/CAR/PDMS), needle size 23 ga, StableFlex, for use with autosampler
Supelco
Gruppo in fibra SPME divinilbenzene/carbossene/polidimetilsilossano (DVB/CAR/PDMS), needle size 24 ga, for use with manual holder
Supelco
Gruppo in fibra SPME divinilbenzene/carbossene/polidimetilsilossano (DVB/CAR/PDMS), needle size 23 ga, StableFlex, for use with manual holder or autosampler, fiber L 2 cm
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Gruppo in fibra SPME divinilbenzene/carbossene/polidimetilsilossano (DVB/CAR/PDMS), needle size 24 ga, StableFlex, for use with autosampler
Supelco
Unità fibra SPME polidimetilsilossano (PDMS), df 100 μm(PDMS, for use with autosampler, needle size 23 ga
Supelco
Unità fibra SPME polidimetilsilossano (PDMS), df 100 μm(PDMS, needle size 24 ga, for use with manual holder
Supelco
Unità fibra SPME polidimetilsilossano (PDMS), df 100 μm(PDMS, for use with autosampler, needle size 24 ga
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Gruppo in fibra SPME carbossene/polidimetilsilossano (CAR/PDMS), df 75 μm(CAR/PDMS, for use with manual holder, needle size 24 ga
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Gruppo fibre SPME polidimetilsilossano/divinilbenzene (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, StableFlex, for use with autosampler
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Gruppo in fibra SPME carbossene/polidimetilsilossano (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 24 ga, StableFlex, for use with autosampler
Supelco
Gruppo fibre SPME polidimetilsilossano/divinilbenzene (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, for use with manual holder
Supelco
Gruppo in fibra SPME carbossene/polidimetilsilossano (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 23 ga, StableFlex, for use with autosampler
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Gruppo fibre SPME poliacrilato (PA), df 85 μm(PA, for use with autosampler, needle size 23 ga
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Gruppo in fibra SPME carbossene/polidimetilsilossano (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 24 ga, for use with autosampler
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Gruppo in fibra SPME carbossene/polidimetilsilossano (CAR/PDMS), df 85 μm(CAR/PDMS, needle size 24 ga, for use with manual holder, StableFlex fiber
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Gruppo fibre SPME polidimetilsilossano/divinilbenzene (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 23 ga, PDMS/DVB StableFlex, for use with autosampler
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Gruppo fibre SPME poliacrilato (PA), df 85 μm(PA, for use with autosampler, needle size 24 ga
Supelco
Gruppo fibre SPME polidimetilsilossano/divinilbenzene (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, for use with autosampler
Supelco
Gruppo fibre SPME polidimetilsilossano/divinilbenzene (PDMS/DVB), df 65 μm(PDMS/DVB, needle size 24 ga, StableFlex, for use with manual holder
Supelco
Gruppo in fibra SPME carbossene/polidimetilsilossano (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 23 ga, for use with autosampler
Supelco
Unità fibra SPME polidimetilsilossano (PDMS), df 100 μm(PDMS, for use with manual holder, needle size 23 ga
Supelco
Gruppo fibre SPME polidimetilsilossano/divinilbenzene (PDMS/DVB), df 65 μm(PDMS/DVB, for use with autosampler, needle size 23 ga
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SPME StableFlex fiber assortment kit, for use with manual holder
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Gruppo in fibra SPME carbossene/polidimetilsilossano (CAR/PDMS), df 75 μm(CAR/PDMS, needle size 23 ga, for use with manual holder
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Gruppo fibre SPME, rivestimento in glicole polietilenico (PEG) Carbowax, needle size 23 ga, df 60 μm(PEG, for use with autosampler
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SPME StableFlex fiber assortment kit, needle size 23 ga, for use with autosampler
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Gruppo fibre SPME polidimetilsilossano/divinilbenzene (PDMS/DVB), fused silica fiber, df 65 μm(PDMS/DVB, for use with manual holder, needle size 23 ga
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Gruppo fibre SPME poliacrilato (PA), df 85 μm(PA, for use with manual holder, needle size 24 ga
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Gruppo in fibra SPME divinilbenzene/carbossene/polidimetilsilossano (DVB/CAR/PDMS), for use with autosampler, needle size 23 ga, metal alloy fiber, fiber L 2 cm