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Fase stazionaria per GC

phase Apiezon L, bottle of 25 g

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About This Item

Codice UNSPSC:
41115717

Forma fisica

solid

Confezionamento

bottle of 25 g

Parametri

50-300 °C temp. range

tecniche

gas chromatography (GC): suitable

Gruppo funzionale matrice

Apiezon L phase

Solubilità

chloroform, toluene: soluble

Tipo di colonna

packed GC

Descrizione generale

GC methods are divided into two classes depending on the nature of stationary phases; gas-solid chromatography (GSC) and gas-liquid chromatography (GLC). GSC has solid adsorptive material and solute particles are removed from mobile phase by electrostatic forces. GLC has a thin layer of liquid coated or bonded on the surface of an inert particle or on the walls of the column where solute particles are retained in the liquid phase based on their partition coefficients. The primary necessity of a stationary phase is to provide sample separation sustaining phase integrity over a reasonable period of time. It should be stable for the chemical and thermal changes. Selectivity, peak symmetry, analysis time, degree of separation and peak tailing are a few parameters which are considered while choosing a stationary phase. Apiezon L is basically purified hydrocarbon grease which is suitable as a liquid phase for GC analysis. It is considered as one of the most selective phase for Polychlorinated Biphenyls (PCB) congeners.
Sintetizzata appositamente per risultare più pura, con range di peso molecolare ristretto e senza impurità o catalizzatori in tracce per l′impiego come fase stazionaria per la GC.

Applicazioni

Apiezon L may be used as stationary phase to determine the retention indices of benzene and benzene derivatives on the basis of their molecular structure using GC equipped with a thermal conductivity detector.

Codice della classe di stoccaggio

13 - Non Combustible Solids

Classe di pericolosità dell'acqua (WGK)

WGK 3

Punto d’infiammabilità (°F)

Not applicable

Punto d’infiammabilità (°C)

Not applicable

Dispositivi di protezione individuale

Eyeshields, Gloves, type N95 (US)


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Mitchell D. Erickson
Analytical Chemistry of PCBs, 250-250 (1997)
Calculation of retention indices for benzene and benzene derivatives on the basis of molecular structure.
Cook, Lawrence E., and Frank M. Raushel.
Journal of Chromatography A, 65, 556-559 (1972)
David B. Troy, Paul Beringer
Remington: The Science and Practice of Pharmacy, 605-605 (2006)
James P. Lodge, Jr.
Methods of Air Sampling and Analysis, 98-98 (1988)

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