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34998

Sigma-Aldrich

Acetonitrile

Acetonitrile
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≥99.9%, HPLC Plus, suitable for IR spectroscopy, HPLC

Sinonimo/i:

ACN, Cianometano, Cianuro di metile, Etilnitrile

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1 L
222,00 €
2.5 L
467,00 €

222,00 €


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Cambia visualizzazione
1 L
222,00 €
2.5 L
467,00 €

About This Item

Formula condensata:
CH3CN
Numero CAS:
Peso molecolare:
41.05
Beilstein:
741857
Numero CE:
Numero MDL:
Codice UNSPSC:
41116105
eCl@ss:
39031501
ID PubChem:
NACRES:
NA.03
Grado:
HPLC Plus
Saggio:
≥99.9%
tecniche:
HPLC: suitable
IR spectroscopy: suitable
applicazioni:
food and beverages
P. ebollizione:
81-82 °C (lit.)
Tensione di vapore:
72.8 mmHg ( 20 °C)

222,00 €


Per informazioni sulla disponibilità, contatta il Servizio Clienti.

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Nome del prodotto

Acetonitrile, HPLC Plus, ≥99.9%

Grado

HPLC Plus

Livello qualitativo

Densità del vapore

1.41 (vs air)

Tensione di vapore

72.8 mmHg ( 20 °C)

Saggio

≥99.9%

Stato

liquid

Temp. autoaccensione

973 °F

Limite di esplosione

16 %

baseline drift measuring range

≤12 mAU (210 nm)

tecniche

HPLC: suitable
IR spectroscopy: suitable

Impurezze

≤0.0001% free alkali (as NH3)
≤0.0002% non-volatile matter
≤0.001% free acid (as CH3COOH)
≤0.01% water (Karl Fischer)
≤0.5 ppb fluorescence (quinine) at 254 nm
≤0.5 ppb fluorescence (quinine) at 365 nm

Residuo alogenato

10 ng/L (as heptachlor epoxide)

Indice di rifrazione

n20/D 1.344 (lit.)

P. ebollizione

81-82 °C (lit.)

Punto di fusione

−45 °C (lit.)

Densità

0.786 g/mL at 25 °C (lit.)

Gradiente HPLC

≤0.2 mAU at 254 nm
≤1 mAU at 210 nm

λ

H2O reference

Assorbanza UV

λ: 195 nm Amax: ≤0.10
λ: 200 nm Amax: ≤0.02
λ: 228 nm Amax: ≤0.005
λ: 235 nm Amax: ≤0.0044
λ: 250 nm Amax: ≤0.0044
λ: 400 nm Amax: ≤0.0044

applicazioni

food and beverages

Formato

neat

Stringa SMILE

CC#N

InChI

1S/C2H3N/c1-2-3/h1H3
WEVYAHXRMPXWCK-UHFFFAOYSA-N

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Descrizione generale

L'acetonitrile (MeCN) viene ampiamente utilizzato come solvente in diversi studi ed possiede un'elevata costante dielettrica (37,5). Le procedure di purificazione necessarie per ottenere i vari gradi di acetonitrile idonei per le diverse applicazioni (polarografia, spettroscopia, ecc.), sono descritte da numerosi ricercatori.[1]

Applicazioni

L′acetonitrile della nuova qualità UPLC Plus è adatto a tutte le applicazioni, tra cui:
spettrometria di massa, HPLC, TLC, GPC, UV, IR, GC, analisi dei residui di pesticidi e sintesi e purificazione di RNA/DNA.
L′acetonitrile viene utilizzato per preparare l′eluente impiegato per la rilevazione mediante HPLC su gradiente del difenilmetano diisocianato, un prodotto della degradazione polimerica.[2]

Nota sulla preparazione

Prodotto filtrato mediante filtro da 0,2 μm

Altre note

Per l'erogazione dei solventi, i contenitori Pure-Pac® II richiedono l′adattatore Micromatic MacroValve Z560723.
Avviso importante
  • L′articolo codice 34998-4X2.5L uscirà di produzione. Ordinare il flacone singolo 34998-2.5L che è identico e ha le stesse esatte specifiche.
  • L′articolo codice 34998-6X1L uscirà di produzione. Ordinare il flacone singolo 34998-1L che è identico e ha le stesse esatte specifiche.

Prodotti consigliati

Scopri i reagenti LiChropur, ideali per analisi HPLC o LC-MS

Note legali

Pure-Pac is a registered trademark of Merck KGaA, Darmstadt, Germany

Pittogrammi

FlameExclamation mark

Avvertenze

Danger

Indicazioni di pericolo

Classi di pericolo

Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Eye Irrit. 2 - Flam. Liq. 2

Codice della classe di stoccaggio

3 - Flammable liquids

Classe di pericolosità dell'acqua (WGK)

WGK 2

Punto d’infiammabilità (°F)

35.6 °F - closed cup

Punto d’infiammabilità (°C)

2.0 °C - closed cup


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Lot/Batch Number

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Acetonitrile for UHPLC-MS LiChrosolv®

Supelco

1.03725

Acetonitrile

H Haugen et al.
Journal of biomedical materials research. Part B, Applied biomaterials, 73(2), 229-237 (2005-03-10)
This article deals with enzyme-induced biodegradation behavior of thermoplastic polyether-urethane (TPU). Porous scaffolds were processed by a new foaming method applied in hot pressing and injection molding. The scaffolds were subsequently gamma sterilized. The samples were incubated with cholesterol esterase
Alexander David Ardianrama et al.
Journal of colloid and interface science, 552, 485-493 (2019-06-04)
Although triangular silver (Ag) nanoplates are intrinsically unstable, this characteristic has been taken advantage of in the development of a novel sensing platform. However, most of these applications have relied on halide ions as etchants. In the current work, we
Purification of acetonitrile.
Walter M and Ramaley L.
Analytical Chemistry, 45(1), 165-166 (1973)
Timo Glatter et al.
Molecular systems biology, 5, 237-237 (2009-01-22)
Protein complexes represent major functional units for the execution of biological processes. Systematic affinity purification coupled with mass spectrometry (AP-MS) yielded a wealth of information on the compendium of protein complexes expressed in Saccharomyces cerevisiae. However, global AP-MS analysis of
Hélène Hall et al.
Brain : a journal of neurology, 137(Pt 9), 2493-2508 (2014-07-27)
The neuropathological substrate of dementia in patients with Parkinson's disease is still under debate, particularly in patients with insufficient alternate neuropathology for other degenerative dementias. In patients with pure Lewy body Parkinson's disease, previous post-mortem studies have shown that dopaminergic

Domande

1–9 di 9 domande  
  1. What kind of container is used for the 4L? Is a photo available?

    1 risposta
    1. This product is packaged in a 4L amber glass bottle with a teflon-lined polypropylene screw cap. Unfortunately, an image is not available.

      Utile?

  2. What kind of container is used for the 20L? Is a photo available?

    1 risposta
    1. This product is packaged in a 20 liter HDPE drum. Please see the picture attached below.

      Utile?

  3. How can I determine the shelf life / expiration / retest date of this product?

    1 risposta
    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/449/386/product-dating-information-mk.pdf

      Utile?

  4. How is shipping temperature determined? And how is it related to the product storage temperature?

    1 risposta
    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

      Utile?

  5. What is the Department of Transportation shipping information for this product?

    1 risposta
    1. Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product.

      Utile?

  6. What are the options for drying solvents?

    1 risposta
    1. Sigma-Aldrich offers a full range of high-purity solvents with extremely low water levels specifically manufactured for moisture sensitive Organic and Biotech applications.  Sigma-Aldrich also carries various drying agents such as molecular sieves, which are typically compatible with organic solvents.

      Utile?

  7. Can you recommend a Solvent Extractor for organics from aqueous solution?

    1 risposta
    1. Solvent extractors are often used for the quantitative extraction of organics from aqueous solutions and separations in immunoassays. The MIXXOR system has been applied successfully in many laboratory solvent extraction operations and is ideal for the rapid screening of alternative solvents for specific extraction problems.

      Utile?

  8. What apparatus do you recommend for HPLC solvent filtration?

    1 risposta
    1. The Sigma-Aldrich Vacuum Filtration Assembly gives you all the components you need including: funnel top, fritted glass funnel support, filtration flask, aluminum clamp, and silicone stopper.  The Acrodisc Syringe Filters offer high quality filtration for analytical samples, certified for HPLC to ensure low extractable and available in a broad range of membranes to meet sample compatibility requirements.

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  9. Who do I contact about larger solvent volume needs?

    1 risposta
    1. Email us at [email protected] or visit Sigma-Aldrich Fine Chemicals for development and manufacturing-scale inquiries: [email protected]

      Utile?

Recensioni

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Contatta l'Assistenza Tecnica.