Regarding KITALYSIS-CN-1KT KitAlysis™ High-Throughput Buchwald-Hartwig Amination Reaction Screening Kit-Pack of 4, there are links to specific usage instructions posted on this page.
https://www.sigmaaldrich.com/product/aldrich/kitalysiscn#product-documentation
These describe reactions carried out at various temperatures (depending on the substrate used), e.g. 60 - 80 degrees C, controlled by the use of a heating bath.
KITALYSIS-CN
KitAlysis™ High-Throughput Buchwald-Hartwig Amination Reaction Screening Kit-Pack of 4
Sinonimo/i:
Amination Screening Kit, Buchwald-Hartwig Amination
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1 KIT
1.340,00 €
1.340,00 €
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Cambia visualizzazione
1 KIT
1.340,00 €
About This Item
Codice UNSPSC:
12161503
NACRES:
NA.22
1.340,00 €
Per informazioni sulla disponibilità, contatta il Servizio Clienti.
Richiedi un ordine bulk
Prodotti consigliati
Impiego in reazioni chimiche
reaction type: Buchwald-Hartwig Amination
reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Cross Couplings
reagent type: catalyst
core: palladium
Temperatura di conservazione
room temp
Descrizione generale
The KitAlysis™ High Throughput Buchwald–Hartwig Amination Reaction Screening Kit enables chemists to quickly and efficiently screen Buchwald–Hartwig C–N cross-coupling reaction conditions. Quick identification of optimal conditions allows faster scale-up of the synthetic reaction. All required chemicals come pre-weighed for ease of use. A step-by-step user guide and experimental excel sheets are available for download to facilitate the process.
Applicazioni
There are four possible screens that can be run based upon the user’s substrates. Step-by-step user guides and a downloadable experimental excel sheets for each screen is provided in the below hyperlinks.
Two Solvents, Weak Base (Cs2CO3)
Download the experimental excel file here
Two Solvents, Strong Base (NaOt-Bu)
Download the experimental excel file here
One Solvent (Dioxane), Two Bases
Download the experimental excel file here
One Solvent (DMAc), Two Bases
Download the experimental excel file here
Each kit contains 4 screening sets that contain the following:
Each customizable screening kit contains
Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).
Two Solvents, Weak Base (Cs2CO3)
Download the experimental excel file here
Two Solvents, Strong Base (NaOt-Bu)
Download the experimental excel file here
One Solvent (Dioxane), Two Bases
Download the experimental excel file here
One Solvent (DMAc), Two Bases
Download the experimental excel file here
Each kit contains 4 screening sets that contain the following:
Each customizable screening kit contains
- 12 X 2 pre-weighed catalysts (1 μmol) in individual microvials with magnetic stir bars
- 2 bases (NaOt-Bu and Cs2CO3)
- 2 degassed anhydrous solvents (dioxane and DMAc) in ampules
- 2 substrate reaction vials with stir bars
- 1 internal standard
- 4 reaction block replacement films
Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).
Caratteristiche e vantaggi
- Designed and tested by synthetic chemists
- Easily run 24-microscale reaction in parallel
- 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration
- Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks
Note legali
KitAlysis is a trademark of Sigma-Aldrich Co. LLC
Solo come componenti del kit
N° Catalogo
Descrizione
- SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA
I componenti del kit sono disponibili anche separatamente
N° Catalogo
Descrizione
SDS
- 900634N,N-Dimethylacetamide, anhydrous, ZerO2®, 99.8% 8 mLSDS
- 9006401,4-Dioxane, anhydrous, ZerO2®, 99.8% 8 mLSDS
- 702706Sodium tert-butoxide solution, 2 M in THF, ZerO2® 4 mLSDS
- 747130Josiphos SL-J009-1 Pd G3 5 µmolSDS
- 753009SPhos Pd G2 5 µmolSDS
- 753246RuPhos Pd G2 5 µmolSDS
- 756482P(t-Bu)3 Pd G2 5 µmolSDS
Vedi tutto (15)
Prodotti correlati
N° Catalogo
Descrizione
Determinazione del prezzo
Raccomandato
N° Catalogo
Descrizione
Determinazione del prezzo
Avvertenze
Danger
Indicazioni di pericolo
Classi di pericolo
Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 1B - Eye Dam. 1 - Repr. 1B - Self-heat. 1 - Skin Corr. 1B - STOT RE 2 Oral - STOT SE 3
Organi bersaglio
Central nervous system, Kidney,Adrenal gland,Testes, Respiratory system
Rischi supp
Codice della classe di stoccaggio
4.2 - Pyrophoric and self-heating hazardous materials
Punto d’infiammabilità (°F)
-4.0 °F - closed cup
Punto d’infiammabilità (°C)
-20 °C - closed cup
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Certificati d'analisi (COA)
Lot/Batch Number
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I clienti hanno visto anche
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Articoli
KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.
Materials Included in your KITALYSIS-24PD-2PK High-Throughput Screening Kit
Preformed catalysts in the kit are stable but become air-sensitive when activated; Schlenk technique aids scale-up.
Protocolli
Protocol for the KitAlysis™ Buchwald-Hartwig Amination Reaction Screening Kit
Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
Catalyst screening kits, KitAlysis™, and TLC-MS analysis enable high-throughput synthesis and analysis for efficient reactions.
KitAlysis™ Cu C-N (Buchwald-Hartwig) cross-coupling high-throughput screening kit. Detailed Set-Up User Guide and a downloadable excel file for calculations.
Contenuto correlato
Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
La progettazione e l’ottimizzazione delle reazioni chimiche in sintesi organica ha lo scopo di modificare in modo preciso i parametri di reazione per il conseguimento di risultati ottimali nella ricerca di vie per ottenere le molecole desiderate.
Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.
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Good morning Iwould have a question regarding the KitAlysis™ High-Throughput Buchwald-Hartwig Amination Reaction Screening Kit-Pack of 4. Is It possible to work at various temperatures or it's only thinked for the RT?
1 risposta-
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