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M-108

Supelco

MTBSTFA

with 1% t-BDMCS, ampule of 5 × 1 mL, analytical standard, Cerilliant®

Synonym(e):

N-Methyl-N-tert-butyldimethylsilyltrifluoracetamid, MTBSTFA + 1 % TBDMSCl, Silylierungsmischung VI

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About This Item

Empirische Formel (Hill-System):
C9H18F3NOSi
CAS-Nummer:
77377-52-7
Molekulargewicht:
241.33
Beilstein:
3606546
MDL-Nummer:
MFCD00009671
UNSPSC-Code:
41116107
PubChem Substanz-ID:
329817850

Produktbezeichnung

N-tert-Butyldimethylsilyl-N-methyltrifluoracetamid mit 1% tert-Butyldimethylchlorsilan, (with 1% t-BDMCS), ampule of 5 × 1 mL, analytical standard, Cerilliant®

Qualität

analytical standard

Qualitätsniveau

100

Eignung der Reaktion

reagent type: derivatization reagent
reaction type: Acylations

Verpackung

ampule of 5 × 1 mL

Hersteller/Markenname

Cerilliant®

Methode(n)

gas chromatography (GC): suitable

Anwendung(en)

forensics and toxicology

Format

neat

Lagertemp.

−20°C

SMILES String

CN(C(=O)C(F)(F)F)[Si](C)(C)C(C)(C)C

InChI

1S/C9H18F3NOSi/c1-8(2,3)15(5,6)13(4)7(14)9(10,11)12/h1-6H3

InChIKey

QRKUHYFDBWGLHJ-UHFFFAOYSA-N

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Anwendung


  • Pharmaceutical substances in ambient particulates: A preliminary assessment.: This study explores the presence of pharmaceutical compounds in environmental particulate matter, using analytical methods that could involve derivatization agents like MTBSTFA. The detection of these substances in air samples suggests potential health impacts and environmental persistence (Cecinato et al., 2017) (Cecinato et al., 2017).


Rechtliche Hinweise

CERILLIANT is a registered trademark of Merck KGaA, Darmstadt, Germany

Piktogramme

FlameExclamation mark
GHS02,GHS07

Signalwort

Warning

Gefahreneinstufungen

Eye Irrit. 2 - Flam. Liq. 3 - Skin Irrit. 2

Lagerklassenschlüssel

3 - Flammable liquids

WGK

WGK 3

Flammpunkt (°F)

113.0 °F - closed cup

Flammpunkt (°C)

45 °C - closed cup

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Analysenzertifikate (COA)

Lot/Batch Number

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Supelco

28564-U

SLB®-5ms GC-Kapillarsäule

O-Methylhydroxylamin -hydrochlorid 98%

Sigma-Aldrich

226904

O-Methylhydroxylamin -hydrochlorid

(±)-MDA-D5 -Lösung 100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

Supelco

M-010

(±)-MDA-D5 -Lösung

Xiaowei Wang et al.
Journal of chromatography. A, 1216(35), 6267-6273 (2009-07-31)
A sample pretreatment method for the determination of 18 chlorophenols (CPs) in aqueous samples by derivatization liquid-phase microextraction (LPME) was investigated using gas chromatography-mass spectrometry. Derivatization reagent was spiked into the extraction solvent to combine derivatization and extraction into one
R Montes et al.
Journal of chromatography. A, 1216(2), 205-210 (2008-12-17)
A fast and novel sample preparation procedure for the determination of triclosan (TCS) and methyltriclosan (MTCS) in water samples is presented. Dispersive liquid-liquid microextraction, using a ternary mixture consisting of a disperser, an extractant and N-methyl-N-(tert-butyldimethylsilyl)trifluoroacetamide (MTBSTFA) as derivatization reagent
Ho-Sang Shin et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 879(7-8), 489-494 (2011-02-01)
A gas chromatography-mass spectrometric (GC-MS) method was developed for the determination of 2-naphthol (2-NAP) and 1-hydroxypyrene (1-HOP) in human urine. Extraction from urine after the enzyme hydrolysis with β-glucuronidase/arylsulfatase was achieved with a liquid extraction using 5 mL of pentane.
Martin Adiels et al.
Rapid communications in mass spectrometry : RCM, 24(5), 586-592 (2010-02-09)
Stable isotope kinetic studies play an important role in the study of very-low density lipoprotein (VLDL) metabolism, including basic and clinical research. Today, [1,1,2,3,3-(2)H(5)]glycerol is the most cost-effective alternative to measure glycerol and triglyceride kinetics. Recycling of glycerol from glycolysis
Stephane Morville et al.
Journal of environmental monitoring : JEM, 6(12), 963-966 (2004-11-30)
A method using GC-MS and derivatization with N-(t-butyldimethylsilyl)-N-methyltrifluoroacetamide (MTBSTFA) was developed for the analysis of 20 phenolic compounds in atmospheric samples (gas and particles). Air sampling was carried out using a Hi-Vol sampler with glass fibre filter and XAD-2 resin
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