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Documentos

79291

Supelco

4-[2-(N,N-Dimethylamino)ethylaminosulfonyl]-7-(2-aminoethylamino)-2,1,3-benzoxadiazole

for HPLC derivatization, LiChropur™, ≥95.0% (HPLC)

Sinônimo(s):

4-[2-(N,N-Dimethylamino)ethylsulfamoyl]-7-(2-aminoethylamino)benzofurazan, 7-[(2-Aminoethyl)amino]-N-[2-(dimethylamino)ethyl]-2,1,3-benzoxadiazole-4-sulfonamide, DAABD-AE

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About This Item

Fórmula empírica (Notação de Hill):
C12H20N6O3S
Número CAS:
913253-56-2
Peso molecular:
328.39
Número MDL:
MFCD21363128
Código UNSPSC:
12000000
ID de substância PubChem:
329768377
NACRES:
NA.22

grau

for HPLC derivatization

Nível de qualidade

100

Ensaio

≥95.0% (HPLC)

forma

powder

qualidade

LiChropur™

prazo de validade

limited shelf life, expiry date on the label

técnica(s)

HPLC: suitable

temperatura de armazenamento

2-8°C

cadeia de caracteres SMILES

CN(C)CCNS(=O)(=O)c1ccc(NCCN)c2nonc12

InChI

1S/C12H20N6O3S/c1-18(2)8-7-15-22(19,20)10-4-3-9(14-6-5-13)11-12(10)17-21-16-11/h3-4,14-15H,5-8,13H2,1-2H3

chave InChI

QKTBJERNSIEPPM-UHFFFAOYSA-N

Categorias relacionadas

Aplicação

4-[2-(N,N-dimethylamino)ethylaminosulfonyl]-7-(2-aminoethylamino)-2,1,3-benzoxadiazole (DAABD-AE) is a new derivatization reagent for rapid and specific liquid chromatography tandem mass spectrometric quantification of pristanic acid, phytanic acid, and very long chain fatty acids (i.e., hexacosanoic, tetracosanoic, and docosanoic acids) in plasma.
4-[2-(N,N-Dimethylamino)ethylaminosulfonyl]-7-(2-aminoethylamino)-2,1,3-benzoxadiazole may be used as derivatization reagent for the trace analysis of carboxylic acids in saliva samples using liquid chromatography-electrospray ionization-tandem mass spectrometry (LC-ESI-MS/MS).

Embalagem

Bottomless glass bottle. Contents are inside inserted fused cone.

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Discover LiChropur reagents ideal for HPLC or LC-MS analysis

Informações legais

LiChropur is a trademark of Merck KGaA, Darmstadt, Germany

Código de classe de armazenamento

11 - Combustible Solids

Classe de risco de água (WGK)

WGK 3

Ponto de fulgor (°F)

Not applicable

Ponto de fulgor (°C)

Not applicable

Choose from one of the most recent versions:

Certificados de análise (COA)

Lot/Batch Number
BCCM2814
BCCL2689
BCCL0516
BCCH2805
BCCF8870

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4-(Dimethylamino)pyridine ReagentPlus®, ≥99%

Sigma-Aldrich

107700

4-(Dimethylamino)pyridine

Perfluorooctanoic acid 95%

Sigma-Aldrich

171468

Perfluorooctanoic acid

Cloreto de dansila suitable for fluorescence, BioReagent, ≥99.0% (HPLC)

Sigma-Aldrich

39220

Cloreto de dansila

Osama Y Al-Dirbashi et al.
Journal of lipid research, 49(8), 1855-1862 (2008-04-29)
Quantification of pristanic acid, phytanic acid, and very long chain fatty acids (i.e., hexacosanoic, tetracosanoic, and docosanoic acids) in plasma is the primary method for investigateing a multitude of peroxisomal disorders (PDs). Typically based on GC-MS, existing methods are time-consuming
Yuhki Tsukamoto et al.
Biomedical chromatography : BMC, 19(10), 802-808 (2005-06-15)
The derivatization regents for carboxylic acids, DAABD-AE (4-[2-(N,N-dimethylamino)ethylaminosulfonyl]7-(2-aminoethylamino)-2,1,3-benzoxadiazole), MePZBD-AE ([4-(4-N-methyl)piperazinosulfonyl]-7-(2-aminoethylamino)-2,1,3-benzoxadiazole) and APZBD-NHMe ([4-(4-N-aminoethyl)piperazinosulfonyl]-7-methylamino-2,1,3-benzoxadiazole) were developed for electrospray ionization-mass spectrometry (ESI-MS). The derivatization reaction with fatty acids was completed at 60 degrees C within 30 min. The derivatives of fatty acids
Milene Volpato et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 1055-1056, 125-134 (2017-05-04)
As pre-clinical and clinical research interest in ω-3 polyunsaturated fatty acids (PUFA) increases, so does the need for a fast, accurate and reproducible analytical method to measure fatty acids (FA) in biological samples in order to validate potential prognostic and
Tatsuya Higashi et al.
Journal of pharmaceutical and biomedical analysis, 52(5), 809-818 (2010-04-09)
A simple and practical derivatization procedure for increasing the detection responses of carboxylic acids in liquid chromatography-electrospray ionization-tandem mass spectrometry (LC-ESI-MS/MS) has been developed. 2-Hydrazinopyridine (HP) and 2-picolylamine (PA) rapidly reacted with biologically and clinically important carboxylic acids [chenodeoxycholic acid

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