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Z744035

Sigma-Aldrich

Penn PhD Photoreactor M2

同義詞:

photoreactor

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About This Item

分類程式碼代碼:
12161600
NACRES:
NA.21
暫時無法取得訂價和供貨情況

AC/DC 輸入

100 - 240 V AC, 50/60 Hz

特點

thermocouple type K-Type Thermocouple
(Touch Screen: 3.5” TFT LCD; 320 x 480 resolution)

反應適用性

reaction type: Photocatalysis
reagent type: catalyst

參數

(Variable stir bar control 100 - 2000 RPM)
0-95% RH at 10-40 °C

寬度 × 高度 × 直徑

11.4 cm × 27.2 cm × 27.9 cm
4.5 in. × 10.7 in. × 11.0 in.

運輸包裝

ambient

相關類別

一般說明

Penn PhD Photoreactor M2是一款台式仪器,专为化学家和研究人员设计,可通过使用光氧化还原催化加速化学反应。 Photoreactor M2将LED照明、机械搅拌和冷却结合到一个设备中。 可用户自定义的温度、强度、搅拌速度和时间参数为创建可重复性、可追溯性、效率和结果一致性提供了有价值的工具。 Photoreactor M2可简化合成序列,并为解决药物开发中分子构建的一些难题提供了重要策略。

特点和优势

  • 模块化设计使得设备可用于各种波长: 450 nm(已包括)、420 nm(需单独购买)、395 nm(需单独购买)和365 nm(需单独购买
  • 360 度反射环境最大程度提高表面光子俘获
  • 光护罩联锁防止用户接触有害光线
  • 互动式触摸屏控制反应参数
  • 通过Intertek ETL、CE和CB许可
  • 用户定义的参数包括温度、光强度、风扇速度和搅拌
  • 自动停止、暂停和重置选项
  • 支持尺寸gc、4、8、20、40 ml的西林瓶
  • 多瓶支架允许同时运行四个8 mL小瓶和五个4 mL小瓶反应。
  • 采用k型热电偶实现温度反馈
可提供区域性插头类型
  • Z744035-1EA-US: B型
  • Z744035-1EA- IN: D型
  • Z744035-1EA-EU-E: E型
  • Z744035-1EA-EU-F: F
  • Z744035-1EA-UK: G型
  • Z744035-1EA-CN: I型
  • Z744035-1EA-CH: J型

光催化技术亮点

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文章

This review provides a summary of recent approaches in developing green methods for visible-light-mediated reactions that operate under mild conditions and avoid the need for toxic transition-metal catalysts or harsh reaction conditions.

Photoredox catalysis is a powerful synthetic methodology to form challenging covalent bonds using light irradiation. It is effective for light-driven polymer and small molecule synthesis.

Effective Csp2- and Csp-hybridized coupling reactions established for catalysis, expanding to multi-step Csp3-coupling.

自由基化学在有机合成中的应用已经过充分发展且影响广泛,但常常受制于对有毒自由基引发剂的依赖。

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Questions

1–4 of 4 Questions  
  1. How is shipping temperature determined? And how is it related to the product storage temperature?

    1 answer
    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

      Helpful?

  2. How can I determine the shelf life / expiration / retest date of this product?

    1 answer
    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/449/386/product-dating-information-mk.pdf

      Helpful?

  3. Is it possible to use this wavelength to photocrosslink polymers, with polyvinyl alcohol, cellulose, lignin, proteins, polysulfone, polyetherimide, etc? If not this equipment, what would be the most appropriate? Thank you. Appreciate your attention.

    1 answer
    1. This product is supplied with the 450 nm light source. Other light sources for this device are available to purchase separately. The following link may be beneficial for you to see how the Penn PhD photoreactor M2 is used in the literature and to describe our different photoreactors.
      https://www.sigmaaldrich.com/US/en/technical-documents/technical-article/chemistry-and-synthesis/photocatalysis/visible-light-photoredox-catalysis

      In addition, please see the link below to review the User Manual for this product:
      https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/product/documents/212/357/photoreactor-m2-user-manual.pdf

      The applications for photoredox catalysis are targeting cross-coupling, C-H functionalization, alkene and arene functionalization, and trifluoromethylation. Additional helpful information may be found by searching popular literature sources such as Google Scholar or PubMed to see if there is a certain cross linking agent that is used for each of the described polymer. It is unclear what type of cross linking functionalization is intended.

      To further discuss, we kindly ask you to navigate to the link https://www.sigmaaldrich.com/techservice, click on "Product Technical Inquires" under the Products Section with all the required information so that a member of our team can reach out to you to assist further. Thank you.

      Helpful?

  4. How exchangeable are the different diodes? Is always only one diode insyalled? Please send a full quatation with all the optipons

    1 answer
    1. The diodes are fixed and not interchangeable. See the link below to review the product user guide:
      https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/product/documents/212/357/photoreactor-m2-user-manual.pdf

      In reference to the quote request, this can be supplied by our Sales team who can assist you further. We kindly ask you to navigate to the link https://www.sigmaaldrich.com/techservice, click on "Quotes" under the Orders section with all the required information so that a member of our team can reach out to you to assist further. Thank you.

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