Regarding KITALYSIS-CN-1KT KitAlysis™ High-Throughput Buchwald-Hartwig Amination Reaction Screening Kit-Pack of 4, there are links to specific usage instructions posted on this page.
https://www.sigmaaldrich.com/product/aldrich/kitalysiscn#product-documentation
These describe reactions carried out at various temperatures (depending on the substrate used), e.g. 60 - 80 degrees C, controlled by the use of a heating bath.
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反应适用性
reaction type: Buchwald-Hartwig Amination
reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Cross Couplings
reagent type: catalyst
core: palladium
储存温度
room temp
一般描述
KitAlysis™高通量Buchwald–Hartwig氨化反应筛选试剂盒可帮助化学家快速而有效地筛选Buchwald–Hartwig C–N交叉耦合反应条件。快速确定最佳条件，使合成反应能够更快地扩展。所有必需化学品均已预先称重，易于使用。可下载逐步用户指南和实验电子表格，加快进程。
应用
根据用户’的底物，可以运行四种可能的筛选。以下超链接为用户提供了分步操作指南和可下载的为每次筛选设计的实验excel表格。
两种溶剂，弱碱（Cs2CO3）
在此处下载实验excel文件
两种溶剂，强碱（NaOt-Bu）
在此处下载实验excel文件
一种溶剂（二恶烷），两种碱
在此处下载实验excel文件
一种溶剂（DMAc），两种碱
在此处下载实验excel文件
每个试剂盒中包含4组筛选，包括以下内容：
每个可定制的筛选套件包含
使用KitAlysis效果最佳 B台式插入盒 和 24-孔反应块 （单独销售）。
两种溶剂，弱碱（Cs2CO3）
在此处下载实验excel文件
两种溶剂，强碱（NaOt-Bu）
在此处下载实验excel文件
一种溶剂（二恶烷），两种碱
在此处下载实验excel文件
一种溶剂（DMAc），两种碱
在此处下载实验excel文件
每个试剂盒中包含4组筛选，包括以下内容：
每个可定制的筛选套件包含
- 12 X 2每个预称重的催化剂 (1 μmol) 在带有磁性搅拌棒的单个小瓶中
- 2种碱(NaOt-Bu and Cs2CO3)
- 2个装在安瓿瓶中的脱气无水溶剂（二氧六环和DMAc）
- 2 个带有搅拌棒的底物反应瓶
- 1 个内标
- 4个反应遮挡可替换膜
使用KitAlysis效果最佳 B台式插入盒 和 24-孔反应块 （单独销售）。
特点和优势
- 由合成化学家设计和测试
- 轻松平行运行 24 个微型反应
- 含 1 μmol 催化剂、3 当量碱、0.1 M 浓度的 10μmol 反应
- 可定制的 Excel 模板，可快速计算，并易于整合到电子实验室笔记本中
法律信息
KitAlysis is a trademark of Sigma-Aldrich Co. LLC
仅试剂盒组分
产品编号
说明
- SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA
试剂盒组分也可单独购买
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价格
警示用语：
Danger
危险分类
Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 1B - Eye Dam. 1 - Repr. 1B - Self-heat. 1 - Skin Corr. 1B - STOT RE 2 Oral - STOT SE 3
靶器官
Central nervous system, Kidney,Adrenal gland,Testes, Respiratory system
补充剂危害
储存分类代码
4.2 - Pyrophoric and self-heating hazardous materials
闪点(°F)
-4.0 °F - closed cup
闪点(°C)
-20 °C - closed cup
其他客户在看
High-Throughput Experimentation in Catalysis and Materials Science.
Gordillo A, et al. et al.
Ullmann's Encyclopedia of Industrial Chemistry (2014)
Spencer D Dreher et al.
Journal of the American Chemical Society, 130(29), 9257-9259 (2008-06-28)
Microscale parallel experimentation was used to discover three catalyst systems capable of coupling secondary organotrifluoroborates with sterically and electronically demanding aryl chlorides and bromides. The ensuing results represent the first comprehensive study of alkylboron coupling to aryl chlorides and, in
Scientist-Led High-Throughput Experimentation (HTE) and Its Utility in Academia and Industry.
Schmink JR, et al.
Aldrichimica Acta, 46, 71-80 (2013)
Karl D Collins et al.
Nature chemistry, 6(10), 859-871 (2014-09-23)
New organic reactivity has often been discovered by happenstance. Several recent research efforts have attempted to leverage this to discover new reactions. In this Review, we attempt to unify reported approaches to reaction discovery on the basis of the practical
实验方案
Protocol for the KitAlysis™ Buchwald-Hartwig Amination Reaction Screening Kit
Protocol for the KitAlysis™ Buchwald-Hartwig Amination Reaction Screening Kit
Protocol for the KitAlysis™ Buchwald-Hartwig Amination Reaction Screening Kit
Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
相关内容
Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
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Good morning Iwould have a question regarding the KitAlysis™ High-Throughput Buchwald-Hartwig Amination Reaction Screening Kit-Pack of 4. Is It possible to work at various temperatures or it's only thinked for the RT?
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