KITALYSIS-PHO

KitAlysis^™ High-Throughput 24-Catalyst Photoredox Reaction Screening Kit-Pack of 2

• Synonym(e): high-throughput photoredox catalyst screening kit
• UNSPSC-Code: 12161600
• NACRES: NA.22

Eigenschaften

• Eignung der Reaktion: reagent type: catalyst; reaction type: Photocatalysis

Beschreibung

Anwendung

Screening kit for photocatalytic reactions to be used with Photo KitAlysis Starter Kit. Step-by-step user guide is provided in the below hyperlink.
Step-by-Step Guide for Photocatalysis Reaction Screening Kit
Downloadable experimental excel file

Each kit contains 2 customizable screening sets that include the following components:

• 24 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat
• 4 degassed anhydrous solvents (DCM, DCE, DMF, MeCN)
• 1 NEW KitAlysis 24-Well Reaction Block Replacement Film
• 4 empty substrate stock solution reaction vials with stirbars
• 1 internal standard

For use Photo KitAlysis High-Throughput Screen Platform (sold seperately)

• Photo KitAlysis Starter Kit with Blue LED Array (470 nm)
• Green LED Array (527 nm)
• White LED Array

Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box (sold separately).

Features:

• Designed and tested by synthetic chemists
• Easily run 24-microscale reactions in parallel
• 10 μmol reactions with 1 μmol catalyst, 0.1 M concentration
• Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks

Rechtliche Hinweise

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Kit-Komponenten auch einzeln erhältlich

• 224758 Tris(2,2′-bipyridyl)dichlororuthenium(II) hexahydrate, powder
• 232017 Tetrachloro-1,4-benzoquinone, 99%
• 272345 2,4,6-Triphenylpyrylium tetrafluoroborate, 98%
• 318337 Acridine Orange hydrochloride hydrate, ≥98% (HPLC)
• 333190 Bismuth(III) sulfide, 99%
• 343714 Dichlorotris(1,10-phenanthroline)ruthenium(II) hydrate, 98%
• 459852 9,10-Anthracenedicarbonitrile, 97%
46955 Fluorescein, for fluorescence, free acid
637017 Bismuth(III) oxide, nanopowder, 90-210 nm particle size, 99.8% trace metals basis
688096 Tris[2-phenylpyridinato-C²,N]iridium(III), 97%
747769 [Ir(dtbbpy)(ppy)₂]PF₆
747777 [Ru(bpz)₃][PF₆]₂, 95%
747785 [Ru(bpm)₃][Cl]₂
747793 (Ir[dF(CF₃)ppy]₂(dtbpy))PF₆
793221 9-Mesityl-10-phenylacridinium tetrafluoroborate
793876 9-Mesityl-2,7-dimethyl-10-phenylacridinium tetrafluoroborate
794171 9-Mesityl-10-methylacridinium tetrafluoroborate
804215 [Ir{dFCF₃ppy}₂(bpy)]PF₆
900421 9-Mesityl-3,6-di-tert-butyl-10-phenylacridinium tetrafluoroborate, ≥95%
900692 2,4,6-Tris(4-methoxyphenyl)pyrylium tetrafluoroborate
900693 9-Mesityl-1,3,6,8-tetramethoxy-10-phenylacridin-10-ium tetrafluoroborate, 95%
900694 10-(3,5-Dimethoxyphenyl)-9-mesityl-1,3,6,8-tetramethoxyacridin-10-ium tetrafluoroborate, ≥93%
D60400 2,3-Dichloro-5,6-dicyano-p-benzoquinone, 98%
P2508 Proflavine hemisulfate salt hydrate, powder
900633 Dichloromethane, anhydrous, contains 40-150 ppm amylene as stabilizer, ZerO₂^®, ≥99.8%
900637 1,2-Dichloroethane, anhydrous, ZerO₂^®, 99.8%
900638 N,N-Dimethylformamide, anhydrous, ZerO₂^®, 99.8%
900644 Acetonitrile, anhydrous, ZerO₂^®, 99.8%
B34656 Biphenyl, ReagentPlus^®, 99.5%
Z118850 Spinbar^® magnetic stirring fleas, red, L 10 mm, diam. 3 mm

Alle anzeigen (30)

Sicherheitshinweise

• Piktogramme: GHS02,GHS06,GHS08,GHS05,GHS09
• Signalwort: Danger
• H-Sätze: H225,H301 + H331,H304,H312,H315,H317,H318,H335,H336,H341,H350,H360D,H373,H410
• P-Sätze: P210 - P273 - P280 - P301 + P310 - P305 + P351 + P338 - P331
• Gefahreneinstufungen: Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Acute Tox. 4 Dermal - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Carc. 1B - Eye Dam. 1 - Flam. Liq. 2 - Muta. 2 - Repr. 1B - Skin Irrit. 2 - Skin Sens. 1 - STOT RE 2 Oral - STOT SE 3
• Zielorgane: Central nervous system, Kidney, Respiratory system
• Zusätzliche Gefahrenhinweise: EUH029
• Lagerklassenschlüssel: 3 - Flammable liquids
• WGK: WGK 3
• Flammpunkt (°F): 35.6 °F - closed cup
• Flammpunkt (°C): 2.0 °C - closed cup