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Documenti

M-108

Supelco

MTBSTFA

with 1% t-BDMCS, ampule of 5 × 1 mL, analytical standard, Cerilliant®

Sinonimo/i:

N-tert-Butyldimethylsilyl-N-methyltrifluoroacetamide with 1% tert-Butyldimethylchlorosilane, N-Methyl-N-tert-butyldimethylsilyltrifluoroacetamide, MTBSTFA + 1% TBDMSCl, Silylating mixture VI

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About This Item

Formula empirica (notazione di Hill):
C9H18F3NOSi
Numero CAS:
77377-52-7
Peso molecolare:
241.33
Beilstein:
3606546
Numero MDL:
MFCD00009671
Codice UNSPSC:
41116107
ID PubChem:
329817850

product name

MTBSTFA (with 1% t-BDMCS), (with 1% t-BDMCS), ampule of 5 × 1 mL, analytical standard, Cerilliant®

Grado

analytical standard

Impiego in reazioni chimiche

reagent type: derivatization reagent
reaction type: Acylations

Confezionamento

ampule of 5 × 1 mL

Produttore/marchio commerciale

Cerilliant®

tecniche

gas chromatography (GC): suitable

applicazioni

forensics and toxicology

Formato

neat

Temperatura di conservazione

−20°C

Stringa SMILE

CN(C(=O)C(F)(F)F)[Si](C)(C)C(C)(C)C

InChI

1S/C9H18F3NOSi/c1-8(2,3)15(5,6)13(4)7(14)9(10,11)12/h1-6H3
QRKUHYFDBWGLHJ-UHFFFAOYSA-N

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Applicazioni


  • Pharmaceutical substances in ambient particulates: A preliminary assessment.: This study explores the presence of pharmaceutical compounds in environmental particulate matter, using analytical methods that could involve derivatization agents like MTBSTFA. The detection of these substances in air samples suggests potential health impacts and environmental persistence (Cecinato et al., 2017) (Cecinato et al., 2017).


Note legali

CERILLIANT is a registered trademark of Merck KGaA, Darmstadt, Germany

Pittogrammi

FlameExclamation mark
GHS02,GHS07

Avvertenze

Warning

Indicazioni di pericolo

H226,H315,H319

Classi di pericolo

Eye Irrit. 2 - Flam. Liq. 3 - Skin Irrit. 2

Codice della classe di stoccaggio

3 - Flammable liquids

Classe di pericolosità dell'acqua (WGK)

WGK 3

Punto d’infiammabilità (°F)

113.0 °F - closed cup

Punto d’infiammabilità (°C)

45 °C - closed cup

Certificati d'analisi (COA)

Cerca il Certificati d'analisi (COA) digitando il numero di lotto/batch corrispondente. I numeri di lotto o di batch sono stampati sull'etichetta dei prodotti dopo la parola ‘Lotto’ o ‘Batch’.

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Sigma-Aldrich

226904

Methoxyamine hydrochloride

(±)-MDA-D5 solution 100 μg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

Supelco

M-010

(±)-MDA-D5 solution

José Angel Prieto et al.
Clinical biochemistry, 42(1-2), 125-128 (2008-11-11)
Evaluation of a GC-MS method using N-tert-butyldimethylsilyl-N-methyltrifluoroacetamide (MTBSTFA) as the silylating agent for GC-MS. Study of the stability of creatine and guanidinoacetate in urine. 22 urines were kept at RT, 4 degrees C and -30 degrees C for 15 days.
P Canosa et al.
Journal of chromatography. A, 1072(1), 107-115 (2005-05-11)
A solid-phase microextraction (SPME) method for the determination of triclosan, methyl triclosan, 2,4-dichlorophenol and 2,3,4-trichlorophenol (considered as possible triclosan metabolites) in water samples was optimised. Analytes were first concentrated on a SPME fibre, directly exposed to the sample, and then
Paul L Wood et al.
Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 831(1-2), 313-319 (2006-01-13)
The GC-MS quantitation of a large number of neurochemicals utilizing a single derivatization step is not common but is provided by the reagent N-(tert-butyldimethylsilyl)-N-methyltrifluro-acetamide (MTBSTFA). Previous workers have utilized this derivative for GC-MS analyses of amino acids, carboxylic acids and
Clayton B'Hymer et al.
Analytical and bioanalytical chemistry, 383(2), 201-209 (2005-09-15)
Several extraction and derivatization procedures were evaluated for the quantification of (2-methoxyethoxy)acetic acid (MEAA) in urine. MEAA is a metabolite and a biomarker for exposure to 2-(2-methoxyethoxy)ethanol, a glycol ether with widespread use in various industrial applications and the specific
Xiaowei Wang et al.
Journal of chromatography. A, 1216(35), 6267-6273 (2009-07-31)
A sample pretreatment method for the determination of 18 chlorophenols (CPs) in aqueous samples by derivatization liquid-phase microextraction (LPME) was investigated using gas chromatography-mass spectrometry. Derivatization reagent was spiked into the extraction solvent to combine derivatization and extraction into one
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