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2,4-Dinitrobenzenesulfonic acid hydrate

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About This Item

Fórmula linear:
(O2N)2C6H3SO3H · xH2O
Número CAS:
698999-22-3
Peso molecular:
248.17 (anhydrous basis)
Número MDL:
MFCD00066017
Código UNSPSC:
12352100
ID de substância PubChem:
24879598
NACRES:
NA.22

pf

95-98 °C (lit.)

grupo funcional

nitro
sulfonic acid

cadeia de caracteres SMILES

OS(=O)(=O)c1ccc(cc1[N+]([O-])=O)[N+]([O-])=O

InChI

1S/C6H4N2O7S/c9-7(10)4-1-2-6(16(13,14)15)5(3-4)8(11)12/h1-3H,(H,13,14,15)

chave InChI

OVOJUAKDTOOXRF-UHFFFAOYSA-N

Aplicação

2,4-Dinitrobenzenesulfonic acid hydrate may be used in the synthesis of the corresponding α-hydroxyketone. It can be used as a catalyst in the amidation reaction, which involves the conversion of secondary-benzylic alcohols to N-benzylacetamides.[1] It may also be used to prepare 1-octyl-2-pyrrolidinonium 2,4-dinitrobenzenesulfonate ([NOP][DNBSA]), a Brønsted-acidic ionic liquid, which can catalyze the synthesis of trioxane.[2]

Pictogramas

Corrosion
GHS05

Palavra indicadora

Danger

Frases de perigo

H314

Classificações de perigo

Skin Corr. 1B

Código de classe de armazenamento

8A - Combustible corrosive hazardous materials

Classe de risco de água (WGK)

WGK 3

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Certificados de análise (COA)

Lot/Batch Number
MKCM8197
MKCQ7618
MKCQ2262
MKCN6225
STBH2928

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"The Ritter reaction under truly catalytic Bronsted acid conditions"
Sanz R, et al.
European Journal of Organic Chemistry, 2007(08), 4642-4645 (2007)
"Bronsted-Acidic Ionic Liquids as Catalysts for Synthesizing Trioxane"
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  1. How is shipping temperature determined? And how is it related to the product storage temperature?

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    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

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    1 answer

    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/449/386/product-dating-information-mk.pdf

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