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Merck

28471-U

Supelco

SLB®-5ms GC-Kapillarsäule

L × I.D. 30 m × 0.25 mm, df 0.25 μm

Synonym(e):

GC column, SPB-5, 5% diphenyl, mass spec

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About This Item

UNSPSC-Code:
12000000
eCl@ss:
32119290
NACRES:
SB.54

Materialien

fused silica

Agentur

Standard Method 6040D
EN 2005/108/EC
EPA 610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA
EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST
JMHLW
NIOSH 2530,5503
OSHA 62
meets requirements for USP G27 and G36
suitable for EPA 1613

Einhaltung gesetzlicher Vorschriften

FDA LIB 4423

Parameter

-60-340 °C temperature (isothermal)
-60-360 °C temperature (programmed)

Beta-Wert

250

df

0.25 μm

Methode(n)

GC/MS: suitable
gas chromatography (GC): suitable

L × ID

30 m × 0.25 mm

Aktive Matrixgruppe

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase

Anwendung(en)

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
industrial hygiene
life science and biopharma
personal care
petroleum
pharmaceutical (small molecule)

Säulenart

capillary non-polar

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Allgemeine Beschreibung

Anwendung: Die zu 5 % Phenyl äquivalente Phase sorgt für eine Siedepunkt-basierte Elutionsordnung mit einer leichten Erhöhung der Selektivität, insbesondere bei aromatischen Verbindungen. Aufgrund der geringen Ausblutung, Trägheit und Beständigkeit wird diese Säule bei Umweltanalyten (wie schwerflüchtigen Stoffen, Pestiziden, PCBs und Herbiziden) bzw. bei jeglichen Anwendungen, für die eine unpolare Säule mit geringer Ausblutung benötigt wird, bevorzugt verwendet.
USP-Code: Diese Säule erfüllt die Anforderungen von USP G27 und G36.
Phase:
  • Gebunden und hoch vernetzt
  • Das Silphenylen-Polymer ist hinsichtlich seiner Polarität nahezu äquivalent zu Poly(5%-Diphenyl/95%-Dimethylsiloxan)
Temperatur- grenzwerte:
  • ≤0,32 mm ID: -60 °C bis 340 °C (isotherm) oder 360 °C (programmiert)
  • ≥0,53 mm ID: -60 °C bis 330 °C (isotherm) oder 340 °C (programmiert)

Anwendung


  • Determination of propargite, tebuconazole and bromopropylate pesticide residues in Taiwan green jujubes by gas chromatography-tandem mass spectrometry.: This study utilized the SLB-5ms Capillary GC Column to analyze pesticide residues in agricultural produce. The method demonstrated high sensitivity and specificity, highlighting the column′s efficacy in complex sample matrices (Zhang et al., 2014).

  • Characterisation of capillary ionic liquid columns for gas chromatography-mass spectrometry analysis of fatty acid methyl esters.: The research explored the performance of SLB-5ms Capillary GC Columns for the analysis of fatty acid methyl esters. The column exhibited superior resolution and stability, making it a valuable tool for lipid analysis in biochemical applications (Zeng et al., 2013).

Sonstige Hinweise

Wir haben eine Reihe von Chromatografiezubehör im Angebot, einschließlich analytische Spritzen

Rechtliche Hinweise

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany

Anwendung

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Die Dokumentenbibliothek aufrufen

Tommy W McGaha et al.
PloS one, 10(3), e0118904-e0118904 (2015-03-19)
The suite of pheromones that promote communal oviposition by Simulium vittatum, a North American black fly species, was identified and characterized using gas chromatography-mass spectrometry, electrophysiological, and behavioral bioassays. Behavioral assays demonstrated that communal oviposition was induced by egg-derived compounds
Chemical Characterization of Three Accessions of Brassica juncea L. Extracts from Different Plant Tissues
Oulad El Majdoub Y, et al.
Molecules (Basel), 25(22), 5421-5421 (2020)
Lorenzo Cucinotta et al.
Journal of chromatography. A, 1655, 462473-462473 (2021-09-01)
The use of IRMS as a GC detector has a history going back decades, however the critical issue of wrong δ13C measurements resulting from impure peaks has been often underestimated. To this regard, multidimensional separation techniques are effective tools to
Sophie Duclos et al.
Proteomics, 11(5), 854-864 (2011-02-01)
The essential roles of the endovacuolar system in health and disease call for the development of new tools allowing a better understanding of the complex molecular machinery involved in endocytic processes. We took advantage of the floating properties of small
Rasha M Faty et al.
Molecules (Basel, Switzerland), 20(2), 1842-1859 (2015-01-28)
Bromination of N-substituted homophthalimides and tetrahydropyrido[4,3-d]- pyrimidine-5,7-diones produces 4,4-dibromohomophthalimide and 8,8-dibromo-tetrahydropyrido[4,3-d]pyrimidine-5,7-dione derivatives, respectively, that can be used as precursors for spiro derivatives. The dibromo derivatives react with different binucleophilic reagents to produce several spiroisoquinoline and spirotetrahydropyrido[4,3-d]- pyrimidine-5,7-dione derivatives, respectively. Reaction

Artikel

Resolving by Mass

GC Analysis of Neroli Essential Oil on SLB®-5ms

Learn more about how the thermal desorption technique is applied for terpene identification, profiling, odor measurement, industrial hygiene, and environmental emissions.

Sigma-Aldrich presents an article about the analysis of melamine and related compounds in dog food with the use of more economical gas chromatography-mass spectrometry (GC-MS) instrumentation.

Alle anzeigen

Protokolle

GC Analysis of PBDE Flame-Retardant Compounds

Extraction and Analysis of PAHs in Olive Oil using Molecularly Imprinted Polymer SPE and GC-MS

Example displays how MSTFA/MSTFA-d9 derivatization of amphetamine provides valuable information in mass spectra and chromatograms using SLB-5ms GC column.

There are three types of analyses: GRO, DRO, and TPH. The published methods are simply variations of these to meet the different analytical needs of the individual agencies.

Chromatograms

suitable for GCsuitable for GC, application for SPMEsuitable for GC, application for SPMEsuitable for GCMehr anzeigen

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