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技術
gas chromatography (GC): suitable
測試參數
sample/matrix: each analyte at 50 ppb in 5 mL water
purge trap: VOCARB 3000 “K”
purge: 40 mL/min at 25 °C for 11 min
dry purge: 2 min
desorption preheat: 205 °C
desorption process: 40 mL/min at 210 °C for 2 min
bake: 260 °C for 10 min
transfer line/valve temp.: 110 °C
column: SPB-624, 30 m × 0.25 mm I.D., 1.4 μm (24255)
oven: 40 °C (2 min), 7 °C/min to 135 °C, 30 °C/min to 230 °C (3 min)
inj. temp.: 150 °C
MSD interface: 200 °C
scan range: m/z = 35-400
carrier gas: helium, 1.1 mL/min
injection: 30:1 split
liner: 0.75 mm I.D. SPME
應用
environmental
法律資訊
SPB is a registered trademark of Merck KGaA, Darmstadt, Germany
分析物
描述
Chloromethane
Vinyl chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
1,1-Dichloroethylene
Dichloromethane
trans-1,2-Dichloroethylene
1,1-Dichloroethane
Chloroform
Dibromofluoromethane
1,1,1-Trichloroethane
Carbon tetrachloride
1,2-Dichloroethane-d4
Benzene
1,2-Dichloroethane
Fluorobenzene
Trichloroethylene
1,2-Dichloropropane
Bromodichloromethane
2-Chloroethyl vinyl ether
cis-1,3-Dichloropropene
Toluene-d8
Toluene
trans-1,3-Dichloropropene
1,1,2-Trichloroethane
Tetrachloroethylene
Dibromochloromethane
Chlorobenzene-d5
Chlorobenzene
Ethylbenzene
Bromoform
4-Bromofluorobenzene
1,1,2,2-Tetrachloroethane
1,3-Dichlorobenzene
1,4-Dichlorobenzene-d4
1,4-Dichlorobenzene
1,2-Dichlorobenzene
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