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重要文件

922668

Sigma-Aldrich

Dichloromeldrum′s acid

≥95%

同義詞:

5,5-Dichloro-2,2-dimethyl-1,3-dioxane-4,6-dione, DiCMA, Lennox-Heard chloroacetylation reagent

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About This Item

經驗公式(希爾表示法):
C6H6Cl2O4
CAS號碼:
分子量::
213.02
MDL號碼:
分類程式碼代碼:
12352106
NACRES:
NA.22
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品質等級

化驗

≥95%

形狀

chunks

mp

51-54 °C

官能基

chloro
ester
ketal

應用

Lennox-Heard reagent (also known as dichloromeldrum′s acid, or DiCMA) is a stable, shelf-stable reagent for the conversion of alkyl and aryl amines to dichloroacetamides. This reagent is atom economical and the byproducts of acetone and CO2 are easily removed, and provides a greener, practical method of installing these medicinally relevant motifs onto a variety of compounds in high yield.

儲存類別代碼

11 - Combustible Solids

水污染物質分類(WGK)

WGK 3

閃點(°F)

Not applicable

閃點(°C)

Not applicable


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David M Heard et al.
Organic letters, 23(9), 3368-3372 (2021-04-13)
Dichloromeldrum's acid is introduced as a bench-stable, nonvolatile reagent for the dichloroacetylation of anilines and alkyl amines to produce α,α-dichloroacetamides, which are important motifs for medicinal chemistry. Products are formed in good to excellent yields with reagent grade solvents, and

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