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Merck
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主要文件

1.14291

Supelco

乙腈

≥99.8% (GC), HPLC grade, isocratic grade, suitable for HPLC, LiChrosolv®

别名:

ACN, 乙腈, 氰甲烷, 甲基氰

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About This Item

线性分子式:
CH3CN
CAS号:
分子量:
41.05
Beilstein:
741857
MDL编号:
UNSPSC代码:
12191502
EC索引号:
200-835-2
NACRES:
NA.03
产品1.14291监管中,请联系销售询价或购买 联系技术服务部门

产品名称

乙腈, isocratic grade for liquid chromatography LiChrosolv®

等级

HPLC grade

质量水平

蒸汽密度

1.41 (vs air)

蒸汽压

72.8 mmHg ( 20 °C)
97 hPa ( 20 °C)

描述

isocratic

产品线

LiChrosolv®

方案

≥99.8% (GC)

表单

liquid

自燃温度

524 °C
973 °F

expl. lim.

16 %

技术

HPLC: suitable

杂质

≤0.0002 meq/g Alkalinity
≤0.0005 meq/g Acidity
≤0.05% Water

蒸发残留物

≤4.0 mg/L

透射比

195 nm, ≥70%
200 nm, ≥90%
240 nm, ≥98%

折射率

n20/D 1.344 (lit.)

沸点

81-82 °C (lit.)

mp

−45 °C (lit.)

转变温度

flash point 2 °C

密度

0.786 g/mL at 25 °C (lit.)

包装形式

neat

储存温度

2-30°C

SMILES字符串

CC#N

InChI

1S/C2H3N/c1-2-3/h1H3

InChI key

WEVYAHXRMPXWCK-UHFFFAOYSA-N

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一般描述

LiChrosolv® 溶剂具有较高的紫外线透射率、低颗粒数、低酸碱度和低蒸发残留量,因而其是可重现分离的理想选择。由于分析型HPLC分离通常在梯度条件下进行,因此我们提供适用的“梯度级”和“等度级”溶剂。这使得所使用的溶剂的梯度影响最小化。

应用

乙腈可用作以下反应的溶剂:
  • 反相高效液相色谱(RP-HPLC)法中的流动性[1]
  • 在等度模式的反相HPLC中用于测定含辣椒和咖喱食品中的苏丹染料。[2]

特点和优势

  • 已通过0.2 µm滤膜过滤
  • 高分离度、灵敏度和优化的色谱峰基线分离

制备说明

产品已经过0.2 μm过滤器过滤

分析说明

纯度 (GC): ≥ 99.8 %
同一性(IR):符合
蒸发残留物: ≤ 4.0 mg/l
水: ≤ 0.05%
酸度: ≤ 0.0005 meq/g
碱度: ≤ 0.0002 meq/g
透射率(195 nm): ≥ 70%
透射率(200 nm): ≥ 90 %
透射率(从240起 nm开始): ≥ 98%
经0.2 µm过滤器过滤

其他说明

欢迎探索各式各样的实验室安全配件和设备,以安全操作溶剂,在首次使用时就能获得较高的安全水平。

法律信息

LICHROSOLV is a registered trademark of Merck KGaA, Darmstadt, Germany

象形图

FlameExclamation mark

警示用语:

Danger

危险分类

Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Eye Irrit. 2 - Flam. Liq. 2

储存分类代码

3 - Flammable liquids

WGK

WGK 2

闪点(°F)

35.6 °F - closed cup

闪点(°C)

2.0 °C - closed cup


分析证书(COA)

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Determination of methylparaben, propylparaben, triamcinolone acetonide and its degradation product in a topical cream by RP-HPLC.
L Matysova et al.
Analytical and Bioanalytical Chemistry, 376, 440-443 (2003)
Development of a fast analytical method for the determination of Sudan dyes in chili-and curry-containing foodstuffs by high-performance liquid chromatography- photodiode array detection.
Vanessa C et al.
Journal of Agricultural and Food Chemistry, 54, 639-644 (2006)

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实验方案

Folic acid vs. folate differences and biological activities; implications in fortified foods and supplements for human health.

Questions

1–2 of 2 Questions  
  1. How is shipping temperature determined? And how is it related to the product storage temperature?

    1 answer
    1. Products may be shipped at a different temperature than the recommended long-term storage temperature. If the product quality is sensitive to short-term exposure to conditions other than the recommended long-term storage, it will be shipped on wet or dry-ice. If the product quality is NOT affected by short-term exposure to conditions other than the recommended long-term storage, it will be shipped at ambient temperature. As shipping routes are configured for minimum transit times, shipping at ambient temperature helps control shipping costs for our customers. For more information, please refer to the Storage and Transport Conditions document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/316/622/storage-transport-conditions-mk.pdf

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  2. How can I determine the shelf life / expiration / retest date of this product?

    1 answer
    1. If this product has an expiration or retest date, it will be shown on the Certificate of Analysis (COA, CofA). If there is no retest or expiration date listed on the product's COA, we do not have suitable stability data to determine a shelf life. For these products, the only date on the COA will be the release date; a retest, expiration, or use-by-date will not be displayed.
      For all products, we recommend handling per defined conditions as printed in our product literature and website product descriptions. We recommend that products should be routinely inspected by customers to ensure they perform as expected.
      For products without retest or expiration dates, our standard warranty of 1 year from the date of shipment is applicable.
      For more information, please refer to the Product Dating Information document: https://www.sigmaaldrich.com/deepweb/assets/sigmaaldrich/marketing/global/documents/449/386/product-dating-information-mk.pdf

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