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Merck

47118

Supelco

橄榄油

analytical standard

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About This Item

CAS号:
EC 号:
MDL编号:
UNSPSC代码:
12164500
价格与库存信息目前不能提供

等级

analytical standard

质量水平

描述

refined

CofA

current certificate can be downloaded

包装

ampule of 1000 mg

技术

HPLC: suitable
gas chromatography (GC): suitable

密度

0.910 g/cm3

应用

food and beverages

包装形式

neat

官能团

ester
oleic acid

运输

ambient

储存温度

2-30°C

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一般描述

Characterized olive oil samples are available for use as controls or check samples for fatty acid methyl ester (FAME) analyses. These reference materials can be used as qualitative standards. They provide an excellent means of standardizing the lipid procedures and comparing the results to others. Packed in an amber ampule under nitrogen.

应用

Olive oil may be used as an analytical reference standard for the determination of the analyte in milk samples by high performance liquid chromatography technique.[1]
Refer to the product′s Certificate of Analysis for more information on a suitable instrument technique. Contact Technical Service for further support.

生化/生理作用

橄榄油对健康的益处来自于其较高的单不饱和脂肪比例,以及其抗氧化剂成分:羟基酪醇、橄榄苦苷和油橄榄酚。

储存分类代码

10 - Combustible liquids

WGK

awg

闪点(°F)

235.4 °F - closed cup

闪点(°C)

113 °C - closed cup


历史批次信息供参考:

分析证书(COA)

Lot/Batch Number

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Analysis of human milk triacylglycerols by high-performance liquid chromatography with light-scattering detection.
Pons SM, et al.
Journal of Chromatography A (1998)
Analysis of human milk triacylglycerols by high-performance liquid chromatography with light-scattering detection.
Pons SM, et al.
Journal of Chromatography A (1998)
Analysis of human milk triacylglycerols by high-performance liquid chromatography with light-scattering detection.
Pons SM, et al.
Journal of Chromatography A (1998)
Nuno Rodrigues et al.
Food research international (Ottawa, Ont.), 128, 108759-108759 (2020-01-21)
Mediterranean olive heritage richness is poorly characterized. Olive oils from minor cultivars of Northeast-Portugal (Lentisca, Madural, Rebolã, Redondal, Verdeal and Verdeal Transmontana) from centenarian trees were chemical and sensory characterized, aiming to identify autochthonous cultivars capable of producing differentiated olive
María Isabel Alarcón Flores et al.
Food chemistry, 134(4), 2465-2472 (2013-02-28)
In this study a simultaneous determination of several classes of polyphenolic compounds (benzoic acid derivates, cinnamic acid derivates, phenyl ethyl alcohols, flavones and other phenolic acids) in feed oils has been carried out by ultra-high performance liquid chromatography coupled to

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Chromatograms

application for HPLCapplication for HPLC

Questions

1–5 of 5 Questions  
  1. I was wondering, what could be the reason to see the FAME peaks in a highly different ratio? (i.e 16:0 relative abundance is larger then 18:1). The chromatogram peaks are very clear and separated, what FAME derivatization method would you suggest to use?

    1 answer
    1. The product issue you are reporting should be investigated by our Technical Service team who can assist you with further troubleshooting and/or investigation. We kindly ask you to navigate to the link https://www.sigmaaldrich.com/techservice, and click on "Report Product Issues" under the Products Section with all the required information so that a member of our team can reach out to you to assist further. Thank you.

      Helpful?

  2. What capillary column can be used to analyze Product 47118, Olive Oil, after prepared into methyl esters?

    1 answer
    1. We used an SP™-2380 capillary column, L × I.D. 30 m × 0.25 mm, df 0.20 μm (Supelco Product No. 24110-U) to analyze the methyl esters of product 47118 Olive Oil.  The temperature program is 150 °C to 250 °C, increasing at a rate of 4 °C per minute, with helium carrier gas at 20 cm/sec at 150 °C. Use an injection volume of 3 μL, and split of 100:1, and FID detection at 260 °C.

      Helpful?

  3. Is Product 47118, Olive Oil, in the form of methyl esters?

    1 answer
    1. No, Product No. 47118 is olive oil with no modifications. The methyl esters may be prepared (for analysis) by following the procedures outlined in AOAC Method 969.33 or AOCS Method Ce 2-66.

      Helpful?

  4. What is the Department of Transportation shipping information for this product?

    1 answer
    1. Transportation information can be found in Section 14 of the product's (M)SDS.To access the shipping information for this material, use the link on the product detail page for the product.

      Helpful?

  5. How do I obtain a Certificate of Composition for Product 47118, Olive Oil?

    1 answer
    1. The Certificate of Composition for Product No. 47118 is shipped with the product and is not available on our website. If you have misplaced this document, please email [email protected] with the lot number to obtain a copy of the Certificate of Composition.

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