GCによる19-成分殺虫剤混合物の分析、SLB^®-5ms [Fast GC Analysis]

column

SLB-5ms, 10 m × 0.10 mm I.D., 0.10 μm (28465-U)

oven

40 °C (1 min), 80 °C/min to 160 °C, 5 °C/min to 340 °C (2 min)

inj. temp.

280 °C

MSD interface

280 °C

scan range

m/z = 45-470

carrier gas

helium, 0.52 mL/min

injection

0.5 μL, 10:1 split

sample

19-component pesticide mix, each analyte at 0.8-2.0 μg/mL in hexane:acetone (50:50)