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product name
TSKgel® 逆相 HPLC カラム (シリカベース), phase C18 (octadecyl), L × I.D. 25 cm × 4.6 mm, 5 μm particle size
物質
stainless steel
認証
suitable for USP L1
製品種目
TSKgel®
メーカー／製品名
Tosoh ODS-80Tm, 08149
標識化の程度
15% Carbon, monolayer, endcapped
パラメーター
0-100% organic solvent
0-45 °C temperature
1.2 mL/min flow rate
310 bar max. pressure
テクニック
HPLC: suitable
L × 内径
25 cm × 4.6 mm
表面積
425 m2/g
マトリックス
silica particle platform
マトリックス活性基
C18 (octadecyl) phase
粒径
5 μm
ポアサイズ
100 Å pore diameter
使用pH
2.0-7.5
分離法
reversed phase
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詳細
TSKgel ODS-80Tmは、低分子量の薬剤、塩基、ヌクレオシドおよびヌクレオチドの分析に使用される汎用カラムです。一般的な用途には、純度チェックやペプチドマッピングなどがあります。 結合相の微細孔サイズは製品説明の中の番号で表され、この場合、TSKgel ODS-80Tmの公称微細孔サイズは 80 Åです。基材シリカの微細孔サイズは100 Åです。
アプリケーション
TSKgel® ODS-80Tm HPLC Column may be used for the separation of:
- Dehydroacetic acid, benzoic acid, sorbic acid and salicylic acid in cosmetic products during their determination by solid-phase extraction (SPE) followed by analysis using high performance liquid chromatography (HPLC) with ultraviolet (UV) detection.
- Cilostazol and its metabolites in human urine during their determination by liquid-liquid extraction (LLE) followed by analysis using HPLC-UV.
- Heterocyclic amines in food products during their analysis by LC coupled to mass spectrometry with electrospray ionization (ESI-MS), LC combined with tandem mass spectrometry (MS/MS) with ESI, LC coupled to atmospheric pressure chemical ionization (APCI)-MS/MS, LC with UV-diode array detection (DAD), LC with UV-fluorescence detection (FLD) and LC in conjunction with electrochemical detection, etc.
- Rabeprazole and its metabolite, rabeprazole thioether in human plasma samples during their analysis by column switching HPLC with UV detection.
- β-lactam antibiotic, cefaclor during its determination by HPLC-FLD.
物理的形状
Shipped in 70% methanol - 30% water.
法的情報
TSKgel is a registered trademark of Tosoh Corporation
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試験成績書（COA）
Lot/Batch Number
Sorry, we don't have COAs for this product available online at this time.
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Determination of cilostazol and its metabolites in human urine by high performance liquid chromatography.
Tata PNV, et al.
Journal of Pharmaceutical and Biomedical Analysis, 24(3), 381-389 (2001)
Determination of rabeprazole and its active metabolite, rabeprazole thioether in human plasma by column-switching high-performance liquid chromatography and its application to pharmacokinetic study.
Uno T, et al.
Journal of Chromatography. B, Biomedical Sciences and Applications, 824(1-2), 238-243 (2005)
Analysis of heterocyclic amines in food products: interlaboratory studies
Santos FJ, et al.
Journal of Chromatography. B, Biomedical Sciences and Applications, 802(1), 69-78 (2004)
Sensitive determination of a β-lactam antibiotic, cefaclor by liquid chromatography with chemiluminescence detection.
Kai M, et al.
Journal of Pharmaceutical and Biomedical Analysis, 30(6), 1765-1771 (2003)
E Mikami et al.
Journal of pharmaceutical and biomedical analysis, 28(2), 261-267 (2002-04-04)
A high-performance liquid chromatographic (HPLC) method for simultaneous determination of dehydroacetic acid (DHA), benzoic acid (BA), sorbic acid (SOA) and salicylic acid (SA) was developed for application to cosmetic products. Isocratic reversed-phase HPLC was employed for quantitative analysis using tetra-n-butylammonium
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