8.52013

Fmoc-Lys(Z)-OH

Novabiochem^®

• Synonyma: Fmoc-Lys(Z)-OH, N-α-Fmoc-N-ε-benzyloxycarbonyl-L-lysine
• Empirický vzorec (Hillův zápis): C₂₉H₃₀N₂O₆
• Číslo CAS: 86060-82-4
• Molekulová hmotnost: 502.56
• MDL number: MFCD00065662
• UNSPSC Code: 12352209
• NACRES: NA.22

Vlastnosti

• Quality Level: 200
• product line: Novabiochem^®
• assay: ≥95.0% (acidimetric); ≥98% (TLC); ≥98.0% (HPLC)
• form: powder
• reaction suitability: reaction type: Fmoc solid-phase peptide synthesis
• manufacturer/tradename: Novabiochem^®
• mp: 105-115 °C
• application(s): peptide synthesis
• functional group: amine
• storage temp.: 2-30°C
• InChI: 1S/C29H30N2O6/c32-27(33)26(16-8-9-17-30-28(34)36-18-20-10-2-1-3-11-20)31-29(35)37-19-25-23-14-6-4-12-21(23)22-13-5-7-15-24(22)25/h1-7,10-15,25-26H,8-9,16-19H2,(H,30,34)(H,31,35)(H,32,33)/t26-/m0/s1
• InChI key: KRULQRVJXQQPQH-SANMLTNESA-N

Popis

General description

Building block for introduction of lysine amino-acid residues by Fmoc SPPS. The side-chain protecting group is TFA-stable but can be removed by hydrogenation over Pd/C or with strong acids such as TFMSA.

Associated Protocols and Technical Articles
Cleavage and Deprotection Protocols for Fmoc SPPS

Linkage

Replaces: 04-12-1027

Analysis Note

Color (visual): white to slight yellow to beige
Appearance of substance (visual): powder
Identity (IR): passes test
Enantiomeric purity: ≥ 99.5 % (a/a)
Purity (TLC(011A)): ≥ 98 %
Purity (TLC(0811)): ≥ 98 %
Assay (HPLC, area%): ≥ 98.0 % (a/a)
Solubility (1 mmole in 2 ml DMF): clearly soluble
Assay (acidimetric): ≥ 95.0 %
Water (K. F.): ≤ 1.00 %

To see the solvent systems used for TLC of Novabiochem^® products please click here.

Legal Information

Novabiochem is a registered trademark of Merck KGaA, Darmstadt, Germany

Bezpečnostní informace

• Storage Class: 11 - Combustible Solids
• wgk_germany: WGK 3
• flash_point_f: Not applicable
• flash_point_c: Not applicable