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Key Documents

20278

Supelco

Supelite DAX-8

jar of 100 g

Sinônimo(s):

XAD-8

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About This Item

Código UNSPSC:
23151817

forma

solid

embalagem

jar of 100 g

técnica(s)

HPLC: suitable
LPLC: suitable
ion chromatography: suitable

área da superfície

140 m2/g

matriz

acrylic ester

Grupo ativo da matriz

polymer

tamanho de partícula

40-60 mesh

tamanho de poro

~0.79 mL/g pore volume
225 Å mean pore size

densidade

1.09 g/mL at 25 °C (true wet)(lit.)
1.23 g/mL at 25 °C (skeletal)(lit.)

técnica de separação

reversed phase

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Descrição geral

Supelite DAX-8 is a nonfunctionalised resin with strong hydrophobic organic matter endorsed to humic and fulvic acids. It is also referred as polymethylmethacrylate resin.

Aplicação

Supelite DAX-8 was used as an absorbent in:
  • HPLC-SEC fractionation system
  • column chromatography
  • extraction procedure and extracts were analysed using Cary Eclipse fluorescence spectrophotometer
Adsorbent resin with moderate polarity for compounds up to 150,000 MW. Most commonly used for adsorption of fulvic and humic acids, treatment of paper pulp mill waste, and removal of alcohols, surfactants, and colorants from samples.

Nota de preparo

DAX-8 is a salt imbibed resin, which requires some preparation prior to use. In the protocol below, you may use methanol in place of ethanol.
  • First, rinse the adsorbent resin with 2-3 bed volumes (BV) of distilled water.
  • Soak overnight in 2 BV of 95% ethanol.
  • After soaking, the resin is introduced into the column and rinsed with an additional 2 BV of 95% ethanol.
  • Rinse with 2 BV of distilled water to displace the ethanol, followed by 1 BV of 4% (w/v) sodium hydroxide, 2 BV of distilled water, 1 BV 4% (v/v) hydrochloric acid, and finally by distilled water until the pH of the eluent becomes neutral.

Informações legais

Código de classe de armazenamento

11 - Combustible Solids

Classe de risco de água (WGK)

WGK 3

Ponto de fulgor (°F)

Not applicable

Ponto de fulgor (°C)

Not applicable

Equipamento de proteção individual

Eyeshields, Gloves, type N95 (US)


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