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PHR1220

Supelco

Diethanolamine

Pharmaceutical Secondary Standard; Certified Reference Material

Sinônimo(s):

2,2′-Iminodiethanol, Bis(2-hydroxyethyl)amine

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About This Item

Fórmula linear:
HN(CH2CH2OH)2
Número CAS:
111-42-2
Peso molecular:
105.14
Beilstein:
605315
Número CE:
203-868-0
Número MDL:
MFCD00002843
Código UNSPSC:
41116107
ID de substância PubChem:
329823227
NACRES:
NA.24

grau

certified reference material
pharmaceutical secondary standard

Nível de qualidade

300

Agency

traceable to USP 1192808

densidade de vapor

3.6 (vs air)

pressão de vapor

<0.98 atm ( 100 °C)

família API

diethanolamine

Certificado de análise (CofA)

current certificate can be downloaded

temperatura de autoignição

689 °F

Lim. expl.

10.6 %

técnica(s)

HPLC: suitable
gas chromatography (GC): suitable

índice de refração

n20/D 1.477 (lit.)

p.e.

217 °C/150 mmHg (lit.)

pf

28 °C (lit.)

densidade

1.097 g/mL at 25 °C (lit.)

aplicação(ões)

pharmaceutical (small molecule)

Formato

neat

temperatura de armazenamento

2-30°C

cadeia de caracteres SMILES

OCCNCCO

InChI

1S/C4H11NO2/c6-3-1-5-2-4-7/h5-7H,1-4H2

chave InChI

ZBCBWPMODOFKDW-UHFFFAOYSA-N

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Descrição geral

Pharmaceutical secondary standards for application in quality control, provide pharma laboratories and manufacturers with a convenient and cost-effective alternative to the preparation of in-house working standards. Diethanolamine is commonly used as a chemical intermediate and as a surface-active agent in agricultural products, pharmaceutical formulations and cosmetics.[1]

Aplicação

These Secondary Standards are qualified as Certified Reference Materials. These are suitable for use in several analytical applications including but not limited to pharma release testing, pharma method development for qualitative and quantitative analyses, food and beverage quality control testing, and other calibration requirements.

Nota de análise

These secondary standards offer multi-traceability to the USP, EP (PhEur) and BP primary standards, where they are available.

Outras notas

This Certified Reference Material (CRM) is produced and certified in accordance with ISO 17034 and ISO/IEC 17025. All information regarding the use of this CRM can be found on the certificate of analysis.
Ion Mobility: TWCCSN2 value of 119.8 Å2 [M+H]+

The collision cross section (CCS) measurement was provided by Waters Corporation, using the SYNAPT XS mass spectrometer.
For a description and overview of how ion mobility enables the measurement of the CCS of an ion visit ims.waters.com.
Further information on the SYNAPT XS mass spectrometer can be found on the IMS microsite and product webpage.

TWCCS measurements are expected to be within 2% of this reference value.

P/N PHR1220 is part of the Waters Extractables & Leachables UNIFI scientific library which can be downloaded from Waters Marketplace.

Nota de rodapé

To see an example of a Certificate of Analysis for this material enter LRAC3260 in the slot below. This is an example certificate only and may not be the lot that you receive.

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Palavra indicadora

Danger

Classificações de perigo

Acute Tox. 4 Oral - Eye Dam. 1 - Repr. 2 - Skin Irrit. 2 - STOT RE 2 Oral

Órgãos-alvo

Kidney,Liver,Blood

Código de classe de armazenamento

11 - Combustible Solids

Classe de risco de água (WGK)

WGK 2

Ponto de fulgor (°F)

280.4 °F - closed cup

Ponto de fulgor (°C)

138 °C - closed cup

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Certificados de análise (COA)

Lot/Batch Number

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Ecotoxicological evaluation of diethanolamine using a battery of microbiotests
Zurita LJ, et al.
Toxicology in vitro, 19(7), 879-886 (2005)
William Conway et al.
Environmental science & technology, 46(13), 7422-7429 (2012-05-25)
The kinetics of the fast reversible carbamate formation reaction of CO(2)(aq) with a series of substituted cyclic secondary amines as well as the noncyclic secondary amine diethanolamine (DEA) has been investigated using the stopped-flow spectrophotometric technique at 25.0 °C. The
Siou-Yin Chen et al.
Inorganic chemistry, 51(8), 4448-4457 (2012-04-05)
The synthesis, X-ray crystallography, magnetic properties, and high-field electron paramagnetic resonance (HFEPR) of a new heptanuclear manganese complex [Mn(7)(heamp)(6)](ClO(4))(2)·4CH(2)Cl(2)·H(2)O (complex 2), in which heampH(3) is 2-[N,N-di(2-hydroxyethyl)aminomethyl]phenol (compound 1), is reported. Complex 2 has a hexagonal, disk-shaped topology and contains six
S H Zeisel et al.
The Biochemical journal, 232(2), 403-408 (1985-12-01)
An understanding of the biosynthesis and metabolism of dimethylamine (DMA) is important because it is a precursor of dimethylnitrosamine (nitroso-DMA). DMA is the major short-chain aliphatic amine in human and rat urine. DMA is formed from trimethylamine (TMA), which, in
L Jiménez et al.
Bioresource technology, 100(3), 1478-1481 (2008-09-24)
The AOpAZRP bleaching sequence (A is an acid treatment, Op an oxygen and peroxide stage, Z an ozone stage, R a reductive treatment and P a peroxide stage) have been applied to oil palm empty fruit bunches (EFB) soda-anthraquinone and
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