418463
2-Iodobenzoic acid
≥99%, purified by sublimation
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About This Item
Fórmula linear:
IC6H4CO2H
Número CAS:
Peso molecular:
248.02
Beilstein:
1861406
Número CE:
Número MDL:
Código UNSPSC:
12352100
ID de substância PubChem:
Produtos recomendados
Ensaio
≥99%
purificado por
sublimation
pf
160-162 °C (lit.)
cadeia de caracteres SMILES
OC(=O)c1ccccc1I
InChI
1S/C7H5IO2/c8-6-4-2-1-3-5(6)7(9)10/h1-4H,(H,9,10)
chave InChI
CJNZAXGUTKBIHP-UHFFFAOYSA-N
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Descrição geral
2-Iodobenzoic acid is a halogen substituted carboxylic acid.
Aplicação
2-Iodobenzoic acid may be used for the following studies:
- One-pot synthesis of hypervalent iodine reagent in the presence of trichloroisocyanuric acid (oxidant). This reagent is employed for the electrophilic trifluoromethylation reactions.
- Synthesis of 1-arylbenziodoxolones.
- Synthesis of isocoumarin.
- Preparation of 2-iodoxybenzoic acid, using oxone (2KHSO5-KHSO4-K2SO4).
Palavra indicadora
Danger
Frases de perigo
Declarações de precaução
Classificações de perigo
Acute Tox. 4 Oral - Eye Dam. 1 - Skin Irrit. 2 - STOT SE 3
Órgãos-alvo
Respiratory system
Código de classe de armazenamento
11 - Combustible Solids
Classe de risco de água (WGK)
WGK 3
Equipamento de proteção individual
dust mask type N95 (US), Eyeshields, Gloves
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Václav Matoušek et al.
The Journal of organic chemistry, 78(13), 6763-6768 (2013-06-06)
Simplified syntheses suited for large scale preparations of the two hypervalent iodine reagents 1 and 2 for electrophilic trifluoromethylation are reported. In both cases, the stoichiometric oxidants sodium metaperiodate and tert-butyl hypochlorite have been replaced by trichloroisocyanuric acid. Reagent 1
Mekhman S Yusubov et al.
The Journal of organic chemistry, 78(8), 3767-3773 (2013-03-14)
Various 1-arylbenziodoxolones can be conveniently prepared from 2-iodobenzoic acid and arenes by a one-pot procedure using Oxone (2KHSO5·KHSO4·K2SO4) as an inexpensive and environmentally safe oxidant. This procedure is also applicable for the synthesis of the 7-methylbenziodoxolone ring system using 2-iodo-3-methylbenzoic
Hypervalent iodine reagents for the oxidation of alcohols and their application to complex molecule synthesis.
Tohma H and Kita Y.
Advanced Synthesis & Catalysis, 346(2), 111-124 (2004)
Manab Chakravarty et al.
The Journal of organic chemistry, 71(24), 9128-9138 (2006-11-18)
Coupling reactions of allenylphosphonates (OCH(2)CMe(2)CH(2)O)P(O)CH=C=CRR' [R, R' = H (1a), R = H, R' = Me (1b), R = R' = Me (1c)] with aryl iodides, iodophenol, and iodobenzoic acid in the presence of palladium(II) acetate are investigated and compared
R J Duhe et al.
Biochimica et biophysica acta, 1017(1), 70-78 (1990-05-15)
The chloroplast coupling factor 1 complex (CF1) contains an epsilon-subunit which inhibits the CF1 ATPase activity. Chloroform treatment of Chlamydomonas reinhardtii thylakoid membranes solubilizes only forms of the enzyme which apparently lack the delta-subunit. Four interrelated observations are described in
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