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Merck

24036

Supelco

SPB®-5 Kapillar-GC-Säule

L × I.D. 60 m × 0.25 mm, df 0.25 μm

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About This Item

UNSPSC-Code:
41115710
eCl@ss:
32119290

Materialien

fused silica

Agentur

meets requirements for USP G27 and G36

Parameter

-60-320 °C temperature (isothermal or programmed)

Beta-Wert

250

df

0.25 μm

Methode(n)

gas chromatography (GC): suitable

L × ID

60 m × 0.25 mm

Aktive Matrixgruppe

Bonded; poly(5% diphenyl/95% dimethyl siloxane) phase

Säulenart

capillary non-polar

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Allgemeine Beschreibung

Betriebsbedingungen: Chemisch kompatibel mit Wasser und anderen Injektions- Lösungsmitteln. Empfindlich gegenüber starken anorganischen Säuren und Laugen. Die Säulen können mit Lösungsmitteln gespült werden.

Anwendung

SPB®-5 Capillary GC Column was used for speciation of the nitrogen compounds (quantitatively), which are polar and somewhat basic in nature, with chemiluminescence detection. It may also be used as stationary phase for determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography. Furthermore, it may also find application in being used as stationary phase in capillary column gas chromatography for determination of sterols.

Sonstige Hinweise

We offer a variety of chromatography accessories including analytical syringes

Rechtliche Hinweise

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany

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Determination of nivalenol and deoxynivalenol in cereals by electron-capture gas chromatography.
Scott PM
Journal - Association of Official Analytical Chemists, 69 (5), 889-893 (1985)
J M Jurado et al.
Talanta, 106, 14-19 (2013-04-20)
4-Methylsterols and 4,4-dimethylsterols of 47 samples of subcutaneous fat from Iberian pigs reared on two different fattening systems, "Extensive" and "Intensive", have been analyzed by GC-MS and GC-FID. The lipids were extracted by melting the subcutaneous fat in a microwave
V Gajdůsková et al.
Veterinarni medicina, 37(8), 471-478 (1992-08-01)
Occurrence of individual polychlorinated biphenyl (PCB) congeners in the environment, foodstuffs and other biological materials was assessed. Analysis of specific PCB congeners (28, 52, 101, 138, 153, 180), occurring in animal raw materials and foodstuffs most frequently, has been implemented.
O Suzuki et al.
Forensic science international, 46(3), 169-180 (1990-07-01)
Positive-ion electron impact (PIEI), positive-ion chemical ionization (PICI) and negative-ion chemical ionization (NICI) mass spectra of 9 carbamate pesticides are presented. In the PIEI mode, the spectra showed small molecular peaks, intense or base peaks due to M - CH3NHCO
Luisito Cercaci et al.
Journal of chromatography. A, 985(1-2), 211-220 (2003-02-13)
The sterol composition of extra virgin olive oil is very characteristic and, thus, has become a helpful tool to detect adulterations with other vegetable oils. Special attention has been addressed to the separate determination of the free and esterified sterol

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