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US EPA Method 608/8081/OLM04.2 PEST: GC Analysis of Organochlorine Pesticides on SPB®-608

US EPA Method 608/8081/OLM04.2 PEST: GC Analysis of Organochlorine Pesticides on SPB®-608 suitable for GC

Materiales

analytical column

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SPB®-608

L × I.D. 30 m × 0.25 mm, df 0.25 μm

SPB®-608

L × I.D. 30 m × 0.53 mm, df 0.50

Columna para GC capilar Equity -1701

L × I.D. 30 m × 0.25 mm, df 0.25 μm

Columna para GC capilar Equity -1701

L × I.D. 30 m × 0.25 mm, df 1.00 μm

Columna para GC capilar Equity -1701

L × I.D. 30 m × 0.53 mm, df 0.50 μm

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 1.00 μm

SLB®-5ms Capillary GC Column

L × I.D. 15 m × 0.10 mm, df 0.10 μm

For use with

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Wheaton wide-mouth bottle

amber soda-lime glass bottle, capacity 1000 mL, white polypropylene cap, (PTFE faced LDPE liner), case of 12 ea

Optional

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Polyimide Sealing Resin

pkg of 5 g

guard column

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Nonpolar Fused Silica Tubing

L × I.D. 5.0 m × 0.10 mm

Nonpolar Fused Silica Tubing

L × I.D. 5.0 m × 0.25 mm

Nonpolar Fused Silica Tubing

L × I.D. 5.0 m × 0.53 mm

required but not provided

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"Y" GlasSeal Connector, Borosilicate Glass

pkg of 1 ea

"Y" Glassseal Connectors

pkg of 1 ea

"Y" Glassseal Connectors

pkg of 3 ea

standard

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Chlordane

certified reference material, 1000 μg/mL in isooctane

Pesticides Matrix Spike Mix

in methanol (varied), PESTANAL®, analytical standard

Camphechlor solution

certified reference material, 1000 μg/mL in isooctane

Pesticide Surrogate Spike Mix

certified reference material, TraceCERT®, 200 μg/mL each component in acetone, ampule of 1 mL

EPA CLP Organochlorine Pesticide MIx

certified reference material, 2000 μg/mL each component in hexane: toluene (1:1), ampule of 1 mL

CONDITIONS

column

SPB-608, 30 m x 0.25 mm I.D., 0.25 μm (24103-U)

oven

100 °C (2 min), 15 °C/min to 300 °C (5 min)

inj. temp.

250 °C

detector

ECD, 300 °C

carrier gas

helium, 0.9 ml/min, constant flow

injection

2.0 μL, splitless (0.75 min)

liner

4 mm I.D. single taper

sample

chlorinated pesticide standard (cat. No. 46845-U), 50 ppb in methylene chloride

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Legal Information

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany