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GC Analysis of 1-Phenylethanol Enantiomers on Astec® CHIRALDEX B-PM

GC Analysis of 1-Phenylethanol Enantiomers on Astec® CHIRALDEX™ B-PM suitable for GC

Matériaux

Colonne analytique

Réf. du produit
Description
Tarif

Astec® CHIRALDEX B-PM Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.12 μm

Étalon

Réf. du produit
Description
Tarif

(R)-(+)-1-phényléthanol

for chiral derivatization, LiChropur, ≥99.0%

1-Phenylethanol-2,2,2-d3

98 atom % D

1-Phenylethanol-1,2-13C2

99 atom % 13C

1-Phenylethanol

98%

1-Phenyl-d5-ethanol

98 atom % D

(S)-(−)-1-phényléthanol

≥98.5% (sum of enantiomers, GC)

(R)-(+)-1-phényléthanol

≥98.5% (sum of enantiomers, GC)

1-Phenylethan-1,2,2,2-d4-ol

98 atom % D

1-Phenylethanol-d10

98 atom % D

1-Phenylethanol-1-13C

99 atom % 13C

1-Phenylethanol-2-13C

99 atom % 13C, 99% (CP)

1-Phenyl-1-ethanol

5000 μg/mL in ethanol: isopropanol (95:5), analytical standard

(S)-(−)-1-phényléthanol

97%

(R)-1-Phenylethanol

97%

CONDITIONS

column

Astec CHIRALDEX B-PM, 30 m x 0.25 mm I.D., 0.12 μm (76023AST)

oven

120 °C

inj. temp.

250 °C

detector

FID, 250 °C

carrier gas

helium, 24 psi

injection

1 μL, 80:1 split

sample

3 mg/mL in methanol
peak 1: R(+)-1-phenylethanol
peak 2: S(-)-1-phenylethanol

Description

Informations légales

Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIRALDEX is a trademark of Sigma-Aldrich Co. LLC