技術
HPLC: suitable
測試參數
column: CHIROBIOTIC V, 25 cm x 4.6 mm I.D., 5 μm particles (11024AST)
mobile phase: [A] n-hexane; [B] 10% ethanol in n-hexane; (75:25, A:B)
flow rate: 1 mL/min
column temp.: 18 °C
detector: UV, 230 nm
sample: 3,5-tBu-MeOBIPHEP ((6,6′-dimethoxybiphenyl-2,2′-diyl)bis[bis(3,5-di-tert-butylphenyl)phosphine]), 1 mg/mL in ethanol with 5 drops of H2O2 added for oxidation
適合性
application for HPLC
應用
chemicals and industrial polymers
法律資訊
Astec is a registered trademark of Merck KGaA, Darmstadt, Germany
CHIROBIOTIC is a registered trademark of Sigma-Aldrich Co. LLC
分析物
描述
(S)-(6,6′-Dimethoxybiphenyl-2,2′-diyl)bis[bis(3,5-di-tert-butylphenyl)phosphine], ≥97%, optical purity ee: ≥99%
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