G006109

GC Analysis of Sulfur Compounds in Gasoline on SPB^®-1 SULFUR

suitable for GC

属性

• 技术: gas chromatography (GC): suitable
• 试验参数: column: SPB-1 SULFUR, 30 m x 0.32 mm I.D., 4.0 μm (24158); oven: 35 ºC, 5 ºC/min to 200 ºC; inj. temp.: 275 °C; detector: FID, 300 ºC; FPD, 300 ºC; carrier gas: helium, 20 cm/sec; injection: 1 μL 100:1 split; sample: Gasoline
• 应用: petroleum

说明

分析说明

Two issues must be overcome for the analysis of sulfur compounds in fuels. 1) Detection of these compounds in a hydrocarbon sample matrix, and 2) adsorption of these compounds by the column. Sulfur specific detectors, such as a flame photometric detector (FPD), can be used to overcome the first challenge. A low phase ratio column, such as the SPB-1 SULFUR, can be used to overcome the second challenge. This slide shows the analysis of a gasoline sample, in which the column effluent was split to two detectors. The top chromatogram shows the FID response, and the bottom chromatogram shows the FPD response.

法律信息

SPB is a registered trademark of Merck KGaA, Darmstadt, Germany