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Merck
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文件

1.05548

Supelco

HPTLC 铝板, 硅胶 60 F₂₅₄

pkg of 25 sheets, sheet L × W 20 cm × 20 cm, aluminum support

别名:

HPTLC F₂₅₄ Silica Gel Plates

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About This Item

分類程式碼代碼:
41115711
NACRES:
NB.21

材料

aluminum support
silica gel 60 matrix

品質等級

特點

binder Organic Polymer
fluorescent indicator

包裝

pkg of 25 sheets

技術

thin layer chromatography (TLC): suitable

層厚度

200 μm

薄片長度 × 寬度

20 cm × 20 cm

粒徑

5-6 μm

孔徑

60 Å medium pore diameter

儲存溫度

2-30°C

一般說明

25 铝片 20 x 20 cm

應用


  • Novel Validated HPTLC Method for the Analysis of Two Binary Mixtures Containing Tamsulosin Hydrochloride with Antimuscarinic Agents.: This study presents a novel HPTLC method using aluminum sheets and Silica gel 60 F₂₅₄ for analyzing binary mixtures of Tamsulosin Hydrochloride with antimuscarinic agents. This method ensures accurate and efficient separation of the components (El-Kimary et al., 2018).

  • Development and Validation of a High-Performance Thin-Layer Chromatographic Method for the Simultaneous Determination of Two Binary Mixtures Containing Ketorolac Tromethamine with Phenylephrine Hydrochloride and with Febuxostat.: This research developed a validated HPTLC method on aluminum sheets coated with Silica gel 60 F₂₅₄ for simultaneous determination of Ketorolac Tromethamine with Phenylephrine Hydrochloride and with Febuxostat, showcasing high accuracy and precision (El Yazbi et al., 2016).

  • HPTLC Determination of Three Gliptins in Binary Mixtures with Metformin.: The article demonstrates the use of HPTLC aluminum sheets with Silica gel 60 F₂₅₄ for determining three gliptins in binary mixtures with Metformin, emphasizing the method′s efficiency and reliability (El-Kimary et al., 2016).

  • Validated HPLC and HPTLC methods for simultaneous determination of colchicine and khellin in pharmaceutical formulations.: This paper details validated HPTLC methods on aluminum sheets and Silica gel 60 F₂₅₄ for simultaneous determination of colchicine and khellin, providing a robust and accurate analytical approach (Hadad et al., 2013).

聯結

替代品:5548-7; 5548

分析報告

特定表面积(根据BET;5-Pt测量):480 - 540 m²/g
孔体积(N₂-等温线):0.74 - 0.84 ml/g
d 50(激光衍射,尺寸分布):5 - 7 µm
层厚度:150 - 200 µm
每块板的层厚度偏差: ≤ 30 µm
色谱检测:
A)颜色测试
hRf 值
-bleu vif organol,显色试验,亲脂性:
17 - 22
- Ceres Black G,颜色测试,亲脂性:38 - 43
- 紫罗兰色,颜色测试,亲脂性:58 - 64
分离数
-显色试验,亲脂性:
≥ 10.0
B)类固醇测试
hRf 值
-氢化可的松,类固醇测试:
23 - 29
- Reichstein S,类固醇检测:36 - 45
- 氢化可的松,类固醇检测:43 - 52
分离数
-类固醇测试:
≥ 42 - 10.5
在条件性纸上确定的典型值
洗脱剂A)甲苯(45%相对湿度)
洗脱剂B)乙酸乙酯/甲苯(95/+5 v/v;20%相对湿度)

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