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质量水平
方案
97%
折射率
n20/D 1.537 (lit.)
沸点
246-247 °C (lit.)
mp
27-30 °C (lit.)
密度
1.47 g/mL at 25 °C (lit.)
官能团
fluoro
SMILES字符串
Fc1ccccc1S(Cl)(=O)=O
InChI
1S/C6H4ClFO2S/c7-11(9,10)6-4-2-1-3-5(6)8/h1-4H
InChI key
ZSZKAQCISWFDCQ-UHFFFAOYSA-N
一般描述
2-Fluorobenzenesulfonyl chloride, also known as o-fluorobenzenesulfonyl chloride, is a flurinated arylsulfonyl chloride. It can be prepared from o-benzenedisulfonyl fluoride. [1]
应用
2-Fluorobenzenesulfonyl chloride may be used in the preparation of the following furan derivatives:
It may also be used to prepare:
- 2-(2-fluorophenyl)benzofuran[2]
- 2-butyl-5-(2-fluorophenyl)furan[3]
- 2-(2-fluorophenyl)-3,6-dimethyl-4,5,6,7-tetrahydrobenzofuran[3]
It may also be used to prepare:
- 2-fluorobenzenesulfonamide[4]
- methyl 2-{[(2-fluorophenyl)sulfonyl]amino}-5,6,7,8-tetrahydro-1-naphthalenecarboxylate[5]
- potassium fluorobenzene-2-sulfonate[6]
- 1-(2-bromobenzyl)-2-(2-fluorophenyl)pyrrole[7]
警示用语：
Danger
危险声明
危险分类
Eye Dam. 1 - Skin Corr. 1B
储存分类代码
8A - Combustible corrosive hazardous materials
WGK
WGK 3
闪点(°F)
230.0 °F - closed cup
闪点(°C)
110 °C - closed cup
个人防护装备
Faceshields, Gloves, Goggles, type ABEK (EN14387) respirator filter
Regiocontroled Palladium?Catalysed Direct Arylation at Carbon C2 of Benzofurans using Benzenesulfonyl Chlorides as the Coupling Partners.
Loukotova L, et al.
ChemCatChem, 6(5), 1303-1309 (2014)
Water-Soluble Phosphines. 6.1 Tailor-Made Syntheses of Chiral Secondary and Tertiary Phosphines with Sulfonated Aromatic Substituents: Structural and Quantum Chemical Studies.
Bitterer F, et al.
Inorganic Chemistry, 35(14), 4103-4113 (1996)
Discovery and optimization of anthranilic acid sulfonamides as inhibitors of methionine aminopeptidase-2: a structural basis for the reduction of albumin binding.
Sheppard GS, et al.
Journal of Medicinal Chemistry, 49(13), 3832-3849 (2006)
Benzenesulfonyl Chlorides: Alternative Coupling Partners for Regiocontrolled Palladium-Catalyzed Direct Desulfitative 5-Arylation of Furans.
Beladhria A, et al.
Synthesis, 46(18), 2515-2523 (2014)
Potassium fluoride catalyzed fluorodesulfonylations of aryl sulfonyl fluorides.
Van der Puy M.
The Journal of Organic Chemistry, 53(18), 4398-4401 (1988)
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