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方案
98%
mp
160-163 °C (lit.)
溶解性
DMSO: soluble 25 mg/mL, clear, yellow
SMILES字符串
O=C1N(Sc2ccccc2)C(=O)c3ccccc13
InChI
1S/C14H9NO2S/c16-13-11-8-4-5-9-12(11)14(17)15(13)18-10-6-2-1-3-7-10/h1-9H
InChI key
NMHKBABHRKQHOL-UHFFFAOYSA-N
一般描述
N-(Phenylthio)phthalimide is an N-substituted phthalimide. It is used as a sulphenylating agent. The synthesis of N-(phenylthio)phthalimide has been reported.
应用
N-(Phenylthio)phthalimide is suitable reagent used in the synthesis of phenyl (3-trimethoxysilylpropyl)-disulfide. It may be used in the sulfenylation of ylides and β−keto esters.
N-(Phenylthio)phthalimide may be used as sulfenylating agent in the synthesis of the following:
N-(Phenylthio)phthalimide may be used as sulfenylating agent in the synthesis of the following:
- α-phenylthio-ketones and α-phenylthio-aldehydes from aldehydes and ketones
- 3-sulfenyl indoles from indoles
- optically active 3-phenylthiooxindoles from unprotected 3-substituted oxindoles
- N−alkyl-β-phenylsulfenyl-2-acetylbenzimidazole from N−alkyl−2−acetylbenzimidazole
- N−phenylsulfenyl ketimines from oximes or nitro compounds
储存分类代码
11 - Combustible Solids
WGK
WGK 3
闪点(°F)
Not applicable
闪点(°C)
Not applicable
Quaternized chitosan as an efficient catalyst for synthesis of N-alkylthio-phthalimides.
Hu Z and Li S
International Journal of Chemistry (Canadian Center of Science and Education), 2(2), 213-213 (2010)
Indium chloride: a versatile Lewis acid catalyst for the synthesis of 3-sulfenylindoles.
Kumar PP, et al.
Journal of Sulfur Chemistry, 35(4), 356-361 (2014)
Formation, characterization, and sub-50-nm patterning of organosilane monolayers with embedded disulfide bonds: An engineered self-assembled monolayer resist for electron-beam lithography.
Wang X, et al.
Langmuir, 19(23), 9748-9758 (2003)
The use of anhydrous CeCl3 as a catalyst for the synthesis of 3-sulfenyl indoles.
Silveira CC, et al.
Tetrahedron Letters, 51(15), 2014-2016 (2010)
A new facile sulfenylation of 2-acetylbenzimidazoles.
Kumar PP, et al.
Phosphorus, Sulfur, and Silicon and the Related Elements, 189(12), 1775-1779 (2014)
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