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Merck

Synthesis of an amine-oleate derivative using an ionic liquid catalyst.

Journal of agricultural and food chemistry (2009-09-02)
Atanu Biswas, Brajendra K Sharma, Kenneth M Doll, Sevim Z Erhan, Julious L Willett, H N Cheng
ABSTRAKT

A facile (and environmentally friendly) reaction between epoxidized methyl oleate and aniline to produce an oleate-aniline adduct, without the formation of fatty amide, was discovered. This reaction was carried out neat, with a catalytic amount of an ionic liquid. No solvent was used, no byproducts were produced, and the ionic liquid could be recovered and recycled. The reaction products were fully characterized by NMR and GC-MS.

MATERIAŁY
Numer produktu
Marka
Opis produktu

Sigma-Aldrich
Methyl oleate, 99%
Sigma-Aldrich
Methyl oleate, technical grade, 70%
Supelco
Methyl oleate, analytical standard
Supelco
Methyl elaidate, analytical standard
Sigma-Aldrich
Methyl elaidate, ≥99% (capillary GC)