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Merck

LC/MS (TOF) Analysis of 2C Amine Drugs of Abuse on Ascentis® Express HILIC

LC/MS (TOF) Analysis of 2C Amine Drugs of Abuse on Ascentis® Express HILIC application for HPLC

材料

Standard

製品番号
詳細
価格

T-084

2,5-Dimethoxy-4-(n)-propylthiophenethylamine hydrochloride solution

1.0 mg/mL in acetonitrile: water (9:1) (as free base), ampule of 1 mL, certified reference material, Cerilliant®

分析カラム

製品番号
詳細
価格

53934-U

Ascentis® Express HILIC、2.7 μm HPLCカラム

2.7 μm particle size, L × I.D. 5 cm × 2.1 mm

移動相成分

製品番号
詳細
価格

70221

ギ酸アンモニウム

eluent additive for LC-MS, LiChropur™, ≥99.0%

CONDITIONS

column

Ascentis Express HILIC, 5 cm x 2.1 mm I.D., 2.7 μm particles (53934-U)

mobile phase

2 mM ammonium formate in 90:10 (v:v) acetonitrile:water

flow rate

0.4 mL/min

pressure

943 psi (65 bar)

column temp.

35 °C

detector

TOF/MS

injection

2 μL

sample

300 ng/mL in acetonitrile

詳細

アナリシスノート

The 2C amines are a family of illicit, psychedelic phenethylamines. The term "2C" refers to the two carbon atoms between the benzene ring and the amino group in the parent molecular structure. A rapid separation of four 2C amine compounds is shown here on an Ascentis Express HILIC column with TOF-MS detection. Cerilliant CRMs were used to ensure reliable MS identification and quantification.

法的情報

Ascentis is a registered trademark of Merck KGaA, Darmstadt, Germany

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