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Merck

LC/MS Analysis of Cocaine, Cocaethylene, Oxycodone, and Noroxycodone on Discovery® HS F5

LC/MS Analysis of Cocaine, Cocaethylene, Oxycodone, and Noroxycodone on Discovery® HS F5 application for HPLC

材料

分析カラム

製品番号
詳細
価格

Discovery® HS F5 HPLCカラム

3 μm particle size, L × I.D. 5 cm × 2.1 mm

標準

製品番号
詳細
価格

Cocaethylene solution

1.0 mg/mL in acetonitrile, ampule of 1 mL, certified reference material, Cerilliant®

ノルオキシコドン 塩酸塩 溶液

1.0 mg/mL in methanol (as free base), ampule of 1 mL, certified reference material, Cerilliant®

Oxycodone solution

1.0 mg/mL in methanol, ampule of 1 mL, certified reference material, Cerilliant®

CONDITIONS

column

Discovery HS F5, 5 cm x 2.1 mm I.D., 3 μm particles (567500-U)

mobile phase

[A] 10 mM ammonium formate in water, pH 6.8; [B] 10mM ammonium formate in acetonitrile, pH 6.8; (10:90, A:B)

flow rate

0.3 mL/min

column temp.

35 °C

detector

ESI(+)

injection

2 μL

sample

200 ng/mL in 25:75, water:acetonitrile

詳細

法的情報

Discovery is a registered trademark of Merck KGaA, Darmstadt, Germany